Cargando…

N′-[(E)-4-Bromo­benzyl­idene]-1-benzofuran-2-carbohydrazide monohydrate

The title compound, C(16)H(11)BrN(2)O(2)·H(2)O, exists in a trans conformation with respect to the N=C bond [1.2815 (14) Å] and the benzofuran ring system forms a dihedral angle of 2.96 (5)° with the benzene ring. In the crystal, the ketone O atom accepts two O—H⋯O and one C—H⋯O hydrogen bond, and t...

Descripción completa

Detalles Bibliográficos
Autores principales: Fun, Hoong-Kun, Quah, Ching Kheng, Nitinchandra, Kalluraya, Balakrishna, Babu, M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3393932/
https://www.ncbi.nlm.nih.gov/pubmed/22798797
http://dx.doi.org/10.1107/S1600536812026724
_version_ 1782237784939954176
author Fun, Hoong-Kun
Quah, Ching Kheng
Nitinchandra,
Kalluraya, Balakrishna
Babu, M.
author_facet Fun, Hoong-Kun
Quah, Ching Kheng
Nitinchandra,
Kalluraya, Balakrishna
Babu, M.
author_sort Fun, Hoong-Kun
collection PubMed
description The title compound, C(16)H(11)BrN(2)O(2)·H(2)O, exists in a trans conformation with respect to the N=C bond [1.2815 (14) Å] and the benzofuran ring system forms a dihedral angle of 2.96 (5)° with the benzene ring. In the crystal, the ketone O atom accepts two O—H⋯O and one C—H⋯O hydrogen bond, and the water O atom accepts an N—H⋯O inter­action. Together, these lead to infinite layers lying parallel to (100).
format Online
Article
Text
id pubmed-3393932
institution National Center for Biotechnology Information
language English
publishDate 2012
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-33939322012-07-13 N′-[(E)-4-Bromo­benzyl­idene]-1-benzofuran-2-carbohydrazide monohydrate Fun, Hoong-Kun Quah, Ching Kheng Nitinchandra, Kalluraya, Balakrishna Babu, M. Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(16)H(11)BrN(2)O(2)·H(2)O, exists in a trans conformation with respect to the N=C bond [1.2815 (14) Å] and the benzofuran ring system forms a dihedral angle of 2.96 (5)° with the benzene ring. In the crystal, the ketone O atom accepts two O—H⋯O and one C—H⋯O hydrogen bond, and the water O atom accepts an N—H⋯O inter­action. Together, these lead to infinite layers lying parallel to (100). International Union of Crystallography 2012-06-16 /pmc/articles/PMC3393932/ /pubmed/22798797 http://dx.doi.org/10.1107/S1600536812026724 Text en © Fun et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Fun, Hoong-Kun
Quah, Ching Kheng
Nitinchandra,
Kalluraya, Balakrishna
Babu, M.
N′-[(E)-4-Bromo­benzyl­idene]-1-benzofuran-2-carbohydrazide monohydrate
title N′-[(E)-4-Bromo­benzyl­idene]-1-benzofuran-2-carbohydrazide monohydrate
title_full N′-[(E)-4-Bromo­benzyl­idene]-1-benzofuran-2-carbohydrazide monohydrate
title_fullStr N′-[(E)-4-Bromo­benzyl­idene]-1-benzofuran-2-carbohydrazide monohydrate
title_full_unstemmed N′-[(E)-4-Bromo­benzyl­idene]-1-benzofuran-2-carbohydrazide monohydrate
title_short N′-[(E)-4-Bromo­benzyl­idene]-1-benzofuran-2-carbohydrazide monohydrate
title_sort n′-[(e)-4-bromo­benzyl­idene]-1-benzofuran-2-carbohydrazide monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3393932/
https://www.ncbi.nlm.nih.gov/pubmed/22798797
http://dx.doi.org/10.1107/S1600536812026724
work_keys_str_mv AT funhoongkun ne4bromobenzylidene1benzofuran2carbohydrazidemonohydrate
AT quahchingkheng ne4bromobenzylidene1benzofuran2carbohydrazidemonohydrate
AT nitinchandra ne4bromobenzylidene1benzofuran2carbohydrazidemonohydrate
AT kallurayabalakrishna ne4bromobenzylidene1benzofuran2carbohydrazidemonohydrate
AT babum ne4bromobenzylidene1benzofuran2carbohydrazidemonohydrate