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2-Amino-4-(4-methoxyphenyl)-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile 1,4-dioxane hemisolvate
In the crystal structure of the title compound, C(17)H(16)N(2)O(3)·0.5C(4)H(8)O(2), pairs of N—H⋯N hydrogen bonds link molecules into dimers with R (2) (2)(12) motifs, which are connected by N—H⋯O hydrogen bonds, forming a supramolecular array in the ab plane. The 1,4-dioxane ring, which lies abou...
| Autores principales: | , , , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2012
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3393982/ https://www.ncbi.nlm.nih.gov/pubmed/22798847 http://dx.doi.org/10.1107/S1600536812027729 |
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| author | Mohamed, Shaaban K. Akkurt, Mehmet Tahir, Muhammad N. Abdelhamid, Antar A. Younes, Sabry H. H. |
| author_facet | Mohamed, Shaaban K. Akkurt, Mehmet Tahir, Muhammad N. Abdelhamid, Antar A. Younes, Sabry H. H. |
| author_sort | Mohamed, Shaaban K. |
| collection | PubMed |
| description | In the crystal structure of the title compound, C(17)H(16)N(2)O(3)·0.5C(4)H(8)O(2), pairs of N—H⋯N hydrogen bonds link molecules into dimers with R (2) (2)(12) motifs, which are connected by N—H⋯O hydrogen bonds, forming a supramolecular array in the ab plane. The 1,4-dioxane ring, which lies about an inversion center, adopts a chair conformation. |
| format | Online Article Text |
| id | pubmed-3393982 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2012 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-33939822012-07-13 2-Amino-4-(4-methoxyphenyl)-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile 1,4-dioxane hemisolvate Mohamed, Shaaban K. Akkurt, Mehmet Tahir, Muhammad N. Abdelhamid, Antar A. Younes, Sabry H. H. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal structure of the title compound, C(17)H(16)N(2)O(3)·0.5C(4)H(8)O(2), pairs of N—H⋯N hydrogen bonds link molecules into dimers with R (2) (2)(12) motifs, which are connected by N—H⋯O hydrogen bonds, forming a supramolecular array in the ab plane. The 1,4-dioxane ring, which lies about an inversion center, adopts a chair conformation. International Union of Crystallography 2012-06-23 /pmc/articles/PMC3393982/ /pubmed/22798847 http://dx.doi.org/10.1107/S1600536812027729 Text en © Mohamed et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Organic Papers Mohamed, Shaaban K. Akkurt, Mehmet Tahir, Muhammad N. Abdelhamid, Antar A. Younes, Sabry H. H. 2-Amino-4-(4-methoxyphenyl)-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile 1,4-dioxane hemisolvate |
| title | 2-Amino-4-(4-methoxyphenyl)-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile 1,4-dioxane hemisolvate |
| title_full | 2-Amino-4-(4-methoxyphenyl)-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile 1,4-dioxane hemisolvate |
| title_fullStr | 2-Amino-4-(4-methoxyphenyl)-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile 1,4-dioxane hemisolvate |
| title_full_unstemmed | 2-Amino-4-(4-methoxyphenyl)-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile 1,4-dioxane hemisolvate |
| title_short | 2-Amino-4-(4-methoxyphenyl)-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile 1,4-dioxane hemisolvate |
| title_sort | 2-amino-4-(4-methoxyphenyl)-5-oxo-5,6,7,8-tetrahydro-4h-chromene-3-carbonitrile 1,4-dioxane hemisolvate |
| topic | Organic Papers |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3393982/ https://www.ncbi.nlm.nih.gov/pubmed/22798847 http://dx.doi.org/10.1107/S1600536812027729 |
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