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5-Hy­droxy-6-[(E)-2-phenyl­ethen­yl]-5,6-dihydro-2H-pyran-2-one isolated from Goniothalamus ridleyi

In the title compound, C(13)H(12)O(3), the pyran ring adopts a half-chair conformation with a C atom deviating from the least-squares plane of the remaining ring atoms by 0.606 (2) Å. This plane and that of the benzene ring make a dihedral angle of 44.18 (6)°. In the crystal, mol­ecules are linked t...

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Detalles Bibliográficos
Autores principales: Jusoh, Samsiah, Din, Laily B., Zakaria, Zuriati, Khaledi, Hamid
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3394055/
https://www.ncbi.nlm.nih.gov/pubmed/22798920
http://dx.doi.org/10.1107/S1600536812028334
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author Jusoh, Samsiah
Din, Laily B.
Zakaria, Zuriati
Khaledi, Hamid
author_facet Jusoh, Samsiah
Din, Laily B.
Zakaria, Zuriati
Khaledi, Hamid
author_sort Jusoh, Samsiah
collection PubMed
description In the title compound, C(13)H(12)O(3), the pyran ring adopts a half-chair conformation with a C atom deviating from the least-squares plane of the remaining ring atoms by 0.606 (2) Å. This plane and that of the benzene ring make a dihedral angle of 44.18 (6)°. In the crystal, mol­ecules are linked through O—H⋯O hydrogen bonds into infinite chains along the b axis, and these chains are cross-linked by C—H⋯O hydrogen bonded into sheets lying parallel to the bc plane. The layers are further connected via C—H⋯π inter­actions to form a three-dimensional supra­molecular structure.
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spelling pubmed-33940552012-07-13 5-Hy­droxy-6-[(E)-2-phenyl­ethen­yl]-5,6-dihydro-2H-pyran-2-one isolated from Goniothalamus ridleyi Jusoh, Samsiah Din, Laily B. Zakaria, Zuriati Khaledi, Hamid Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(13)H(12)O(3), the pyran ring adopts a half-chair conformation with a C atom deviating from the least-squares plane of the remaining ring atoms by 0.606 (2) Å. This plane and that of the benzene ring make a dihedral angle of 44.18 (6)°. In the crystal, mol­ecules are linked through O—H⋯O hydrogen bonds into infinite chains along the b axis, and these chains are cross-linked by C—H⋯O hydrogen bonded into sheets lying parallel to the bc plane. The layers are further connected via C—H⋯π inter­actions to form a three-dimensional supra­molecular structure. International Union of Crystallography 2012-06-30 /pmc/articles/PMC3394055/ /pubmed/22798920 http://dx.doi.org/10.1107/S1600536812028334 Text en © Jusoh et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Jusoh, Samsiah
Din, Laily B.
Zakaria, Zuriati
Khaledi, Hamid
5-Hy­droxy-6-[(E)-2-phenyl­ethen­yl]-5,6-dihydro-2H-pyran-2-one isolated from Goniothalamus ridleyi
title 5-Hy­droxy-6-[(E)-2-phenyl­ethen­yl]-5,6-dihydro-2H-pyran-2-one isolated from Goniothalamus ridleyi
title_full 5-Hy­droxy-6-[(E)-2-phenyl­ethen­yl]-5,6-dihydro-2H-pyran-2-one isolated from Goniothalamus ridleyi
title_fullStr 5-Hy­droxy-6-[(E)-2-phenyl­ethen­yl]-5,6-dihydro-2H-pyran-2-one isolated from Goniothalamus ridleyi
title_full_unstemmed 5-Hy­droxy-6-[(E)-2-phenyl­ethen­yl]-5,6-dihydro-2H-pyran-2-one isolated from Goniothalamus ridleyi
title_short 5-Hy­droxy-6-[(E)-2-phenyl­ethen­yl]-5,6-dihydro-2H-pyran-2-one isolated from Goniothalamus ridleyi
title_sort 5-hy­droxy-6-[(e)-2-phenyl­ethen­yl]-5,6-dihydro-2h-pyran-2-one isolated from goniothalamus ridleyi
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3394055/
https://www.ncbi.nlm.nih.gov/pubmed/22798920
http://dx.doi.org/10.1107/S1600536812028334
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