(3E,5E)-3,5-Bis(4-methyl­benzyl­idene)-1-[3-(piperidin-1-yl)propano­yl]piperidin-4-one

In the title compound, C(29)H(34)N(2)O(2), the central piperidine ring adopts a half-chair conformation, whereas the terminal one adopts a chair conformation. The mean plane of the central piperidine ring [maximum deviation = 0.384 (2) Å] makes dihedral angles of 64.82 (13) and 17.55 (13)° with the...

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Detalles Bibliográficos
Autores principales: Kia, Yalda, Osman, Hasnah, Murugaiyah, Vikneswaran, Arshad, Suhana, Razak, Ibrahim Abdul
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3414948/
https://www.ncbi.nlm.nih.gov/pubmed/22904935
http://dx.doi.org/10.1107/S1600536812031820
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author Kia, Yalda
Osman, Hasnah
Murugaiyah, Vikneswaran
Arshad, Suhana
Razak, Ibrahim Abdul
author_facet Kia, Yalda
Osman, Hasnah
Murugaiyah, Vikneswaran
Arshad, Suhana
Razak, Ibrahim Abdul
author_sort Kia, Yalda
collection PubMed
description In the title compound, C(29)H(34)N(2)O(2), the central piperidine ring adopts a half-chair conformation, whereas the terminal one adopts a chair conformation. The mean plane of the central piperidine ring [maximum deviation = 0.384 (2) Å] makes dihedral angles of 64.82 (13) and 17.55 (13)° with the benzene rings. In the crystal, mol­ecules are linked into a tape along the b axis via C—H⋯O inter­actions, generating R (2) (2)(20) and R (2) (1)(6) graph-set motifs. C—H⋯π inter­actions are observed between the tapes.
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spelling pubmed-34149482012-08-17 (3E,5E)-3,5-Bis(4-methyl­benzyl­idene)-1-[3-(piperidin-1-yl)propano­yl]piperidin-4-one Kia, Yalda Osman, Hasnah Murugaiyah, Vikneswaran Arshad, Suhana Razak, Ibrahim Abdul Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(29)H(34)N(2)O(2), the central piperidine ring adopts a half-chair conformation, whereas the terminal one adopts a chair conformation. The mean plane of the central piperidine ring [maximum deviation = 0.384 (2) Å] makes dihedral angles of 64.82 (13) and 17.55 (13)° with the benzene rings. In the crystal, mol­ecules are linked into a tape along the b axis via C—H⋯O inter­actions, generating R (2) (2)(20) and R (2) (1)(6) graph-set motifs. C—H⋯π inter­actions are observed between the tapes. International Union of Crystallography 2012-07-18 /pmc/articles/PMC3414948/ /pubmed/22904935 http://dx.doi.org/10.1107/S1600536812031820 Text en © Kia et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Kia, Yalda
Osman, Hasnah
Murugaiyah, Vikneswaran
Arshad, Suhana
Razak, Ibrahim Abdul
(3E,5E)-3,5-Bis(4-methyl­benzyl­idene)-1-[3-(piperidin-1-yl)propano­yl]piperidin-4-one
title (3E,5E)-3,5-Bis(4-methyl­benzyl­idene)-1-[3-(piperidin-1-yl)propano­yl]piperidin-4-one
title_full (3E,5E)-3,5-Bis(4-methyl­benzyl­idene)-1-[3-(piperidin-1-yl)propano­yl]piperidin-4-one
title_fullStr (3E,5E)-3,5-Bis(4-methyl­benzyl­idene)-1-[3-(piperidin-1-yl)propano­yl]piperidin-4-one
title_full_unstemmed (3E,5E)-3,5-Bis(4-methyl­benzyl­idene)-1-[3-(piperidin-1-yl)propano­yl]piperidin-4-one
title_short (3E,5E)-3,5-Bis(4-methyl­benzyl­idene)-1-[3-(piperidin-1-yl)propano­yl]piperidin-4-one
title_sort (3e,5e)-3,5-bis(4-methyl­benzyl­idene)-1-[3-(piperidin-1-yl)propano­yl]piperidin-4-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3414948/
https://www.ncbi.nlm.nih.gov/pubmed/22904935
http://dx.doi.org/10.1107/S1600536812031820
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