2-(Anthracen-9-yl)-10-meth­oxy­benzo[h]quinoline acetone hemisolvate

The asymmetric unit of the title structure, C(28)H(19)NO·0.5C(3)H(6)O, comprises one 2-(anthracen-9-yl)-10-meth­oxy­benzo[h]­quinoline mol­ecule and an acteone mol­ecule with an occupany of 0.5. The solvent mol­ecule is disordered around a centre of symmetry. Its occupancy was determined from NMR da...

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Detalles Bibliográficos
Autores principales: Dong, Zhenming, Liu, Bo, Cui, Xinxin, Liu, Yufang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3414981/
https://www.ncbi.nlm.nih.gov/pubmed/22904968
http://dx.doi.org/10.1107/S1600536812031807
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author Dong, Zhenming
Liu, Bo
Cui, Xinxin
Liu, Yufang
author_facet Dong, Zhenming
Liu, Bo
Cui, Xinxin
Liu, Yufang
author_sort Dong, Zhenming
collection PubMed
description The asymmetric unit of the title structure, C(28)H(19)NO·0.5C(3)H(6)O, comprises one 2-(anthracen-9-yl)-10-meth­oxy­benzo[h]­quinoline mol­ecule and an acteone mol­ecule with an occupany of 0.5. The solvent mol­ecule is disordered around a centre of symmetry. Its occupancy was determined from NMR data and kept fixed during the refinement. The two conjugated ring systems of the mol­ecule are almost perpendicular to each other; the inter­planar angle between the anthracene and quinoline ring systems is 84.9 (2)°.
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spelling pubmed-34149812012-08-17 2-(Anthracen-9-yl)-10-meth­oxy­benzo[h]quinoline acetone hemisolvate Dong, Zhenming Liu, Bo Cui, Xinxin Liu, Yufang Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title structure, C(28)H(19)NO·0.5C(3)H(6)O, comprises one 2-(anthracen-9-yl)-10-meth­oxy­benzo[h]­quinoline mol­ecule and an acteone mol­ecule with an occupany of 0.5. The solvent mol­ecule is disordered around a centre of symmetry. Its occupancy was determined from NMR data and kept fixed during the refinement. The two conjugated ring systems of the mol­ecule are almost perpendicular to each other; the inter­planar angle between the anthracene and quinoline ring systems is 84.9 (2)°. International Union of Crystallography 2012-07-25 /pmc/articles/PMC3414981/ /pubmed/22904968 http://dx.doi.org/10.1107/S1600536812031807 Text en © Dong et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Dong, Zhenming
Liu, Bo
Cui, Xinxin
Liu, Yufang
2-(Anthracen-9-yl)-10-meth­oxy­benzo[h]quinoline acetone hemisolvate
title 2-(Anthracen-9-yl)-10-meth­oxy­benzo[h]quinoline acetone hemisolvate
title_full 2-(Anthracen-9-yl)-10-meth­oxy­benzo[h]quinoline acetone hemisolvate
title_fullStr 2-(Anthracen-9-yl)-10-meth­oxy­benzo[h]quinoline acetone hemisolvate
title_full_unstemmed 2-(Anthracen-9-yl)-10-meth­oxy­benzo[h]quinoline acetone hemisolvate
title_short 2-(Anthracen-9-yl)-10-meth­oxy­benzo[h]quinoline acetone hemisolvate
title_sort 2-(anthracen-9-yl)-10-meth­oxy­benzo[h]quinoline acetone hemisolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3414981/
https://www.ncbi.nlm.nih.gov/pubmed/22904968
http://dx.doi.org/10.1107/S1600536812031807
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AT liuyufang 2anthracen9yl10methoxybenzohquinolineacetonehemisolvate

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