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9-(Thio­phen-2-yl)-8,9-dihydro-3H-pyrazolo­[4,3-f]quinolin-7(6H)-one ethanol monosolvate

In the title compound, C(14)H(11)N(3)OS·C(2)H(5)OH, the dihedral angle between the pyridine N—C(fused)—C(fused)—C(thio­phene) plane and the plane of the thio­phene ring is 81.9 (3)°, indicating that they are close to perpendicular. The dihedral angle between this pyridine plane and the benzene ring...

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Detalles Bibliográficos
Autores principales: Peng, Juhua, Jia, Runhong
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3435639/
https://www.ncbi.nlm.nih.gov/pubmed/22969512
http://dx.doi.org/10.1107/S1600536812033533
Descripción
Sumario:In the title compound, C(14)H(11)N(3)OS·C(2)H(5)OH, the dihedral angle between the pyridine N—C(fused)—C(fused)—C(thio­phene) plane and the plane of the thio­phene ring is 81.9 (3)°, indicating that they are close to perpendicular. The dihedral angle between this pyridine plane and the benzene ring is 1.3 (3)°. The thio­phene ring is disordered over two coplanar orientations with an occupancy ratio of 0.692 (7):0.308 (7), while the ethanol solvent mol­ecule is also disordered over two sets of site in a 0.66 (4):0.34 (4) ratio. In the crystal, chains are formed along the b axis by N—H⋯O and O—H⋯N inter­actions with adjacent chains being connected through C—H⋯N and C—H⋯S inter­actions.