4-Hy­droxy­benzamide 1,4-dioxane hemisolvate

The asymmetric unit of the title compound, C(7)H(7)NO(2)·0.5C(4)H(8)O(2), is composed of one 4-hy­droxy­benzamide mol­ecule and half of a 1,4-dioxane mol­ecule. The complete dioxin molecule is generated by crystallographic inversion symmetry. The crystal has an extensive system of hydrogen bonds, in...

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Detalles Bibliográficos
Autores principales: Tothadi, Srinu, Desiraju, Gautam R.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3435686/
https://www.ncbi.nlm.nih.gov/pubmed/22969557
http://dx.doi.org/10.1107/S160053681203437X
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author Tothadi, Srinu
Desiraju, Gautam R.
author_facet Tothadi, Srinu
Desiraju, Gautam R.
author_sort Tothadi, Srinu
collection PubMed
description The asymmetric unit of the title compound, C(7)H(7)NO(2)·0.5C(4)H(8)O(2), is composed of one 4-hy­droxy­benzamide mol­ecule and half of a 1,4-dioxane mol­ecule. The complete dioxin molecule is generated by crystallographic inversion symmetry. The crystal has an extensive system of hydrogen bonds, in which the three donor H atoms are fully utilized: these result in amide–amide homodimers, and N—H⋯O(dioxane) and O—H⋯O(amide) links.
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spelling pubmed-34356862012-09-11 4-Hy­droxy­benzamide 1,4-dioxane hemisolvate Tothadi, Srinu Desiraju, Gautam R. Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(7)H(7)NO(2)·0.5C(4)H(8)O(2), is composed of one 4-hy­droxy­benzamide mol­ecule and half of a 1,4-dioxane mol­ecule. The complete dioxin molecule is generated by crystallographic inversion symmetry. The crystal has an extensive system of hydrogen bonds, in which the three donor H atoms are fully utilized: these result in amide–amide homodimers, and N—H⋯O(dioxane) and O—H⋯O(amide) links. International Union of Crystallography 2012-08-08 /pmc/articles/PMC3435686/ /pubmed/22969557 http://dx.doi.org/10.1107/S160053681203437X Text en © Tothadi and Desiraju 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Tothadi, Srinu
Desiraju, Gautam R.
4-Hy­droxy­benzamide 1,4-dioxane hemisolvate
title 4-Hy­droxy­benzamide 1,4-dioxane hemisolvate
title_full 4-Hy­droxy­benzamide 1,4-dioxane hemisolvate
title_fullStr 4-Hy­droxy­benzamide 1,4-dioxane hemisolvate
title_full_unstemmed 4-Hy­droxy­benzamide 1,4-dioxane hemisolvate
title_short 4-Hy­droxy­benzamide 1,4-dioxane hemisolvate
title_sort 4-hy­droxy­benzamide 1,4-dioxane hemisolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3435686/
https://www.ncbi.nlm.nih.gov/pubmed/22969557
http://dx.doi.org/10.1107/S160053681203437X
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AT desirajugautamr 4hydroxybenzamide14dioxanehemisolvate

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