2-Benzene­sulfonamido-3-methyl­butyric acid

In the crystal structure of the title compound, C(11)H(15)NO(4)S, two independent mol­ecules are present per asymmetric unit; they are dimerized through O—H⋯O hydrogen bonds between their carb­oxy groups to generate R (2) (2)(8) loops. An intra­molecular N—H⋯O link in one of the mol­ecules closes an...

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Autores principales: Arshad, Muhammad Nadeem, Danish, Muhammad, Tahir, Muhammad Nawaz, Aabideen, Zain Ul, Asiri, Abdullah M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3435689/
https://www.ncbi.nlm.nih.gov/pubmed/22969560
http://dx.doi.org/10.1107/S1600536812034393
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author Arshad, Muhammad Nadeem
Danish, Muhammad
Tahir, Muhammad Nawaz
Aabideen, Zain Ul
Asiri, Abdullah M.
author_facet Arshad, Muhammad Nadeem
Danish, Muhammad
Tahir, Muhammad Nawaz
Aabideen, Zain Ul
Asiri, Abdullah M.
author_sort Arshad, Muhammad Nadeem
collection PubMed
description In the crystal structure of the title compound, C(11)H(15)NO(4)S, two independent mol­ecules are present per asymmetric unit; they are dimerized through O—H⋯O hydrogen bonds between their carb­oxy groups to generate R (2) (2)(8) loops. An intra­molecular N—H⋯O link in one of the mol­ecules closes an S(5) ring. The dimers are linked by N—H⋯O and C—H⋯O hydrogen bonds to form a three-dimensional network. The C atoms of the isopropyl group of one of the mol­ecules are disordered over two orientations in a 3:1 ratio.
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spelling pubmed-34356892012-09-11 2-Benzene­sulfonamido-3-methyl­butyric acid Arshad, Muhammad Nadeem Danish, Muhammad Tahir, Muhammad Nawaz Aabideen, Zain Ul Asiri, Abdullah M. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal structure of the title compound, C(11)H(15)NO(4)S, two independent mol­ecules are present per asymmetric unit; they are dimerized through O—H⋯O hydrogen bonds between their carb­oxy groups to generate R (2) (2)(8) loops. An intra­molecular N—H⋯O link in one of the mol­ecules closes an S(5) ring. The dimers are linked by N—H⋯O and C—H⋯O hydrogen bonds to form a three-dimensional network. The C atoms of the isopropyl group of one of the mol­ecules are disordered over two orientations in a 3:1 ratio. International Union of Crystallography 2012-08-08 /pmc/articles/PMC3435689/ /pubmed/22969560 http://dx.doi.org/10.1107/S1600536812034393 Text en © Arshad et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Arshad, Muhammad Nadeem
Danish, Muhammad
Tahir, Muhammad Nawaz
Aabideen, Zain Ul
Asiri, Abdullah M.
2-Benzene­sulfonamido-3-methyl­butyric acid
title 2-Benzene­sulfonamido-3-methyl­butyric acid
title_full 2-Benzene­sulfonamido-3-methyl­butyric acid
title_fullStr 2-Benzene­sulfonamido-3-methyl­butyric acid
title_full_unstemmed 2-Benzene­sulfonamido-3-methyl­butyric acid
title_short 2-Benzene­sulfonamido-3-methyl­butyric acid
title_sort 2-benzene­sulfonamido-3-methyl­butyric acid
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3435689/
https://www.ncbi.nlm.nih.gov/pubmed/22969560
http://dx.doi.org/10.1107/S1600536812034393
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