Methyl (E)-3,5-dimeth­oxy-2-{[2-(4-meth­oxy­benzo­yl)hydrazin-1-yl­idene]meth­yl}benzoate

In the title compound, C(19)H(20)N(2)O(6), the azomethine [C=N = 1.269 (2) Å] double bond adopts an E conformation and the dihedral angle between the planes of the benzene rings is 17.41 (11)°. In the crystal, inversion dimers linked by pairs of N—H⋯O hydrogen bonds generate R (2) (2)(16) loops. The...

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Autores principales: Naz, Humera, Taha, Muhammad, Rahman, Aqilah Abd, Ismail, Nor Hadiani, Yousuf, Sammer
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3435694/
https://www.ncbi.nlm.nih.gov/pubmed/22969565
http://dx.doi.org/10.1107/S1600536812034782
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author Naz, Humera
Taha, Muhammad
Rahman, Aqilah Abd
Ismail, Nor Hadiani
Yousuf, Sammer
author_facet Naz, Humera
Taha, Muhammad
Rahman, Aqilah Abd
Ismail, Nor Hadiani
Yousuf, Sammer
author_sort Naz, Humera
collection PubMed
description In the title compound, C(19)H(20)N(2)O(6), the azomethine [C=N = 1.269 (2) Å] double bond adopts an E conformation and the dihedral angle between the planes of the benzene rings is 17.41 (11)°. In the crystal, inversion dimers linked by pairs of N—H⋯O hydrogen bonds generate R (2) (2)(16) loops. The dimers are connected by C—H⋯O and C—H⋯N hydrogen bonds, forming sheets lying parallel to (100).
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spelling pubmed-34356942012-09-11 Methyl (E)-3,5-dimeth­oxy-2-{[2-(4-meth­oxy­benzo­yl)hydrazin-1-yl­idene]meth­yl}benzoate Naz, Humera Taha, Muhammad Rahman, Aqilah Abd Ismail, Nor Hadiani Yousuf, Sammer Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(19)H(20)N(2)O(6), the azomethine [C=N = 1.269 (2) Å] double bond adopts an E conformation and the dihedral angle between the planes of the benzene rings is 17.41 (11)°. In the crystal, inversion dimers linked by pairs of N—H⋯O hydrogen bonds generate R (2) (2)(16) loops. The dimers are connected by C—H⋯O and C—H⋯N hydrogen bonds, forming sheets lying parallel to (100). International Union of Crystallography 2012-08-11 /pmc/articles/PMC3435694/ /pubmed/22969565 http://dx.doi.org/10.1107/S1600536812034782 Text en © Naz et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Naz, Humera
Taha, Muhammad
Rahman, Aqilah Abd
Ismail, Nor Hadiani
Yousuf, Sammer
Methyl (E)-3,5-dimeth­oxy-2-{[2-(4-meth­oxy­benzo­yl)hydrazin-1-yl­idene]meth­yl}benzoate
title Methyl (E)-3,5-dimeth­oxy-2-{[2-(4-meth­oxy­benzo­yl)hydrazin-1-yl­idene]meth­yl}benzoate
title_full Methyl (E)-3,5-dimeth­oxy-2-{[2-(4-meth­oxy­benzo­yl)hydrazin-1-yl­idene]meth­yl}benzoate
title_fullStr Methyl (E)-3,5-dimeth­oxy-2-{[2-(4-meth­oxy­benzo­yl)hydrazin-1-yl­idene]meth­yl}benzoate
title_full_unstemmed Methyl (E)-3,5-dimeth­oxy-2-{[2-(4-meth­oxy­benzo­yl)hydrazin-1-yl­idene]meth­yl}benzoate
title_short Methyl (E)-3,5-dimeth­oxy-2-{[2-(4-meth­oxy­benzo­yl)hydrazin-1-yl­idene]meth­yl}benzoate
title_sort methyl (e)-3,5-dimeth­oxy-2-{[2-(4-meth­oxy­benzo­yl)hydrazin-1-yl­idene]meth­yl}benzoate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3435694/
https://www.ncbi.nlm.nih.gov/pubmed/22969565
http://dx.doi.org/10.1107/S1600536812034782
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AT ismailnorhadiani methyle35dimethoxy224methoxybenzoylhydrazin1ylidenemethylbenzoate
AT yousufsammer methyle35dimethoxy224methoxybenzoylhydrazin1ylidenemethylbenzoate

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