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1-[4-(4-Chloro­phen­yl)piperazin-1-yl]-3-(6-oxo-3,4-diphenyl-1,6-dihydro­pyridazin-1-yl)propan-1-one

In the title compound, C(29)H(27)ClN(4)O(2), the six-membered ring of the pyridazine group is nearly planar [maximum deviation = −0.062 (2) Å] and its mean plane makes dihedral angles of 43.05 (9), 44.71 (10) and 72.57 (9)°, respectively, with the two phenyl and benzene rings. The piperazine ring ha...

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Autores principales: Aydın, Abdullah, Akkurt, Mehmet, Doğruer, Deniz S., Büyükgüngör, Orhan
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3435734/
https://www.ncbi.nlm.nih.gov/pubmed/22969605
http://dx.doi.org/10.1107/S160053681203543X
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author Aydın, Abdullah
Akkurt, Mehmet
Doğruer, Deniz S.
Büyükgüngör, Orhan
author_facet Aydın, Abdullah
Akkurt, Mehmet
Doğruer, Deniz S.
Büyükgüngör, Orhan
author_sort Aydın, Abdullah
collection PubMed
description In the title compound, C(29)H(27)ClN(4)O(2), the six-membered ring of the pyridazine group is nearly planar [maximum deviation = −0.062 (2) Å] and its mean plane makes dihedral angles of 43.05 (9), 44.71 (10) and 72.57 (9)°, respectively, with the two phenyl and benzene rings. The piperazine ring has a chair conformation and its mean plane is almost perpendicular to the attached benzene ring, with a dihedral angle of 83.20 (16)°. In the crystal, mol­ecules are linked via two pairs of C—H⋯O inter­actions, which result in the formation of chains propagating along [10-1]. Neighbouring chains are linked via C—H⋯π inter­actions.
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spelling pubmed-34357342012-09-11 1-[4-(4-Chloro­phen­yl)piperazin-1-yl]-3-(6-oxo-3,4-diphenyl-1,6-dihydro­pyridazin-1-yl)propan-1-one Aydın, Abdullah Akkurt, Mehmet Doğruer, Deniz S. Büyükgüngör, Orhan Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(29)H(27)ClN(4)O(2), the six-membered ring of the pyridazine group is nearly planar [maximum deviation = −0.062 (2) Å] and its mean plane makes dihedral angles of 43.05 (9), 44.71 (10) and 72.57 (9)°, respectively, with the two phenyl and benzene rings. The piperazine ring has a chair conformation and its mean plane is almost perpendicular to the attached benzene ring, with a dihedral angle of 83.20 (16)°. In the crystal, mol­ecules are linked via two pairs of C—H⋯O inter­actions, which result in the formation of chains propagating along [10-1]. Neighbouring chains are linked via C—H⋯π inter­actions. International Union of Crystallography 2012-08-15 /pmc/articles/PMC3435734/ /pubmed/22969605 http://dx.doi.org/10.1107/S160053681203543X Text en © Aydın et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Aydın, Abdullah
Akkurt, Mehmet
Doğruer, Deniz S.
Büyükgüngör, Orhan
1-[4-(4-Chloro­phen­yl)piperazin-1-yl]-3-(6-oxo-3,4-diphenyl-1,6-dihydro­pyridazin-1-yl)propan-1-one
title 1-[4-(4-Chloro­phen­yl)piperazin-1-yl]-3-(6-oxo-3,4-diphenyl-1,6-dihydro­pyridazin-1-yl)propan-1-one
title_full 1-[4-(4-Chloro­phen­yl)piperazin-1-yl]-3-(6-oxo-3,4-diphenyl-1,6-dihydro­pyridazin-1-yl)propan-1-one
title_fullStr 1-[4-(4-Chloro­phen­yl)piperazin-1-yl]-3-(6-oxo-3,4-diphenyl-1,6-dihydro­pyridazin-1-yl)propan-1-one
title_full_unstemmed 1-[4-(4-Chloro­phen­yl)piperazin-1-yl]-3-(6-oxo-3,4-diphenyl-1,6-dihydro­pyridazin-1-yl)propan-1-one
title_short 1-[4-(4-Chloro­phen­yl)piperazin-1-yl]-3-(6-oxo-3,4-diphenyl-1,6-dihydro­pyridazin-1-yl)propan-1-one
title_sort 1-[4-(4-chloro­phen­yl)piperazin-1-yl]-3-(6-oxo-3,4-diphenyl-1,6-dihydro­pyridazin-1-yl)propan-1-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3435734/
https://www.ncbi.nlm.nih.gov/pubmed/22969605
http://dx.doi.org/10.1107/S160053681203543X
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