3-(Phenyl­carbamoyl)acrylic acid

In the title compound, C(10)H(9)NO(3), the dihedral angle between the phenyl ring and the amide group is 10.8 (2)°. The C=O and O—H bonds of the carboxyl group adopt an anti orientation and an intra­molecular O—H⋯O hydrogen bond closes an S(7) ring. In the crystal, N—H⋯O hydrogen bonds link the mol­...

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Detalles Bibliográficos
Autores principales: Jin, Shouwen, Huang, Yanfei, Wei, Shuaishuai, Zhou, Yong, Zhou, Yingping
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3435748/
https://www.ncbi.nlm.nih.gov/pubmed/22969619
http://dx.doi.org/10.1107/S1600536812035581
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author Jin, Shouwen
Huang, Yanfei
Wei, Shuaishuai
Zhou, Yong
Zhou, Yingping
author_facet Jin, Shouwen
Huang, Yanfei
Wei, Shuaishuai
Zhou, Yong
Zhou, Yingping
author_sort Jin, Shouwen
collection PubMed
description In the title compound, C(10)H(9)NO(3), the dihedral angle between the phenyl ring and the amide group is 10.8 (2)°. The C=O and O—H bonds of the carboxyl group adopt an anti orientation and an intra­molecular O—H⋯O hydrogen bond closes an S(7) ring. In the crystal, N—H⋯O hydrogen bonds link the mol­ecules into C(7) chains propagating in [101]. The packing is consolidated by C—H⋯O inter­actions, generating sheets aligned at an angle of ca 60° with the bc plane.
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spelling pubmed-34357482012-09-11 3-(Phenyl­carbamoyl)acrylic acid Jin, Shouwen Huang, Yanfei Wei, Shuaishuai Zhou, Yong Zhou, Yingping Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(10)H(9)NO(3), the dihedral angle between the phenyl ring and the amide group is 10.8 (2)°. The C=O and O—H bonds of the carboxyl group adopt an anti orientation and an intra­molecular O—H⋯O hydrogen bond closes an S(7) ring. In the crystal, N—H⋯O hydrogen bonds link the mol­ecules into C(7) chains propagating in [101]. The packing is consolidated by C—H⋯O inter­actions, generating sheets aligned at an angle of ca 60° with the bc plane. International Union of Crystallography 2012-08-23 /pmc/articles/PMC3435748/ /pubmed/22969619 http://dx.doi.org/10.1107/S1600536812035581 Text en © Jin et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Jin, Shouwen
Huang, Yanfei
Wei, Shuaishuai
Zhou, Yong
Zhou, Yingping
3-(Phenyl­carbamoyl)acrylic acid
title 3-(Phenyl­carbamoyl)acrylic acid
title_full 3-(Phenyl­carbamoyl)acrylic acid
title_fullStr 3-(Phenyl­carbamoyl)acrylic acid
title_full_unstemmed 3-(Phenyl­carbamoyl)acrylic acid
title_short 3-(Phenyl­carbamoyl)acrylic acid
title_sort 3-(phenyl­carbamoyl)acrylic acid
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3435748/
https://www.ncbi.nlm.nih.gov/pubmed/22969619
http://dx.doi.org/10.1107/S1600536812035581
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AT huangyanfei 3phenylcarbamoylacrylicacid
AT weishuaishuai 3phenylcarbamoylacrylicacid
AT zhouyong 3phenylcarbamoylacrylicacid
AT zhouyingping 3phenylcarbamoylacrylicacid

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