N-(4-Methyl­phen­yl)-2-nitro­benzene­sulfonamide

In the crystal of the title compound, C(13)H(12)N(2)O(4)S, the conformation of the N—H bond in the –SO(2)—NH– segment is syn to the ortho-nitro group in the sulfonyl benzene ring. The mol­ecule is twisted at the S—N bond with a torsion angle of 76.55 (18)°. The dihedral angle between the planes of t...

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Autores principales: Chaithanya, U., Foro, Sabine, Gowda, B. Thimme
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3435757/
https://www.ncbi.nlm.nih.gov/pubmed/22969628
http://dx.doi.org/10.1107/S1600536812035866
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author Chaithanya, U.
Foro, Sabine
Gowda, B. Thimme
author_facet Chaithanya, U.
Foro, Sabine
Gowda, B. Thimme
author_sort Chaithanya, U.
collection PubMed
description In the crystal of the title compound, C(13)H(12)N(2)O(4)S, the conformation of the N—H bond in the –SO(2)—NH– segment is syn to the ortho-nitro group in the sulfonyl benzene ring. The mol­ecule is twisted at the S—N bond with a torsion angle of 76.55 (18)°. The dihedral angle between the planes of the rings is 72.64 (8)°. In the crystal, mol­ecules are linked by pairs of N—H⋯O(S) hydrogen bonds to form inversion dimers.
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spelling pubmed-34357572012-09-11 N-(4-Methyl­phen­yl)-2-nitro­benzene­sulfonamide Chaithanya, U. Foro, Sabine Gowda, B. Thimme Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal of the title compound, C(13)H(12)N(2)O(4)S, the conformation of the N—H bond in the –SO(2)—NH– segment is syn to the ortho-nitro group in the sulfonyl benzene ring. The mol­ecule is twisted at the S—N bond with a torsion angle of 76.55 (18)°. The dihedral angle between the planes of the rings is 72.64 (8)°. In the crystal, mol­ecules are linked by pairs of N—H⋯O(S) hydrogen bonds to form inversion dimers. International Union of Crystallography 2012-08-23 /pmc/articles/PMC3435757/ /pubmed/22969628 http://dx.doi.org/10.1107/S1600536812035866 Text en © Chaithanya et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Chaithanya, U.
Foro, Sabine
Gowda, B. Thimme
N-(4-Methyl­phen­yl)-2-nitro­benzene­sulfonamide
title N-(4-Methyl­phen­yl)-2-nitro­benzene­sulfonamide
title_full N-(4-Methyl­phen­yl)-2-nitro­benzene­sulfonamide
title_fullStr N-(4-Methyl­phen­yl)-2-nitro­benzene­sulfonamide
title_full_unstemmed N-(4-Methyl­phen­yl)-2-nitro­benzene­sulfonamide
title_short N-(4-Methyl­phen­yl)-2-nitro­benzene­sulfonamide
title_sort n-(4-methyl­phen­yl)-2-nitro­benzene­sulfonamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3435757/
https://www.ncbi.nlm.nih.gov/pubmed/22969628
http://dx.doi.org/10.1107/S1600536812035866
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AT forosabine n4methylphenyl2nitrobenzenesulfonamide
AT gowdabthimme n4methylphenyl2nitrobenzenesulfonamide

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