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(3′R)-3′-Benzyl-2′,3′-dihydro-1H-spiro­[indole-3,1′-naphtho­[2,3-c]pyrrole]-2,4′,9′-trione

In the title compound, C(26)H(18)N(2)O(3), the maximum deviations from planarity for the tetra­hydro-1H-naphtho­[2,3-c]pyrrole and indoline rings systems are 0.091 (1) and 0.012 (2) Å, respectively. These ring systems make a dihedral angle of 89.95 (6)° with each other and they make dihedral angles...

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Autores principales: Sharma, Garima, Kumar, S. Vasanth, Wahab, Habibah A., Rosli, Mohd Mustaqim, Fun, Hoong-Kun
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3435804/
https://www.ncbi.nlm.nih.gov/pubmed/22969650
http://dx.doi.org/10.1107/S1600536812036227
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author Sharma, Garima
Kumar, S. Vasanth
Wahab, Habibah A.
Rosli, Mohd Mustaqim
Fun, Hoong-Kun
author_facet Sharma, Garima
Kumar, S. Vasanth
Wahab, Habibah A.
Rosli, Mohd Mustaqim
Fun, Hoong-Kun
author_sort Sharma, Garima
collection PubMed
description In the title compound, C(26)H(18)N(2)O(3), the maximum deviations from planarity for the tetra­hydro-1H-naphtho­[2,3-c]pyrrole and indoline rings systems are 0.091 (1) and 0.012 (2) Å, respectively. These ring systems make a dihedral angle of 89.95 (6)° with each other and they make dihedral angles of 73.42 (8) and 71.28 (9)°, respectively, with the benzene ring. In the crystal, inversion dimers linked by pairs of N—H⋯O hydrogen bonds generate R (2) (2)(8) loops and C—H⋯O inter­actions connect the dimers into corrugated sheets lying parallel to the bc plane.
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spelling pubmed-34358042012-09-11 (3′R)-3′-Benzyl-2′,3′-dihydro-1H-spiro­[indole-3,1′-naphtho­[2,3-c]pyrrole]-2,4′,9′-trione Sharma, Garima Kumar, S. Vasanth Wahab, Habibah A. Rosli, Mohd Mustaqim Fun, Hoong-Kun Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(26)H(18)N(2)O(3), the maximum deviations from planarity for the tetra­hydro-1H-naphtho­[2,3-c]pyrrole and indoline rings systems are 0.091 (1) and 0.012 (2) Å, respectively. These ring systems make a dihedral angle of 89.95 (6)° with each other and they make dihedral angles of 73.42 (8) and 71.28 (9)°, respectively, with the benzene ring. In the crystal, inversion dimers linked by pairs of N—H⋯O hydrogen bonds generate R (2) (2)(8) loops and C—H⋯O inter­actions connect the dimers into corrugated sheets lying parallel to the bc plane. International Union of Crystallography 2012-08-25 /pmc/articles/PMC3435804/ /pubmed/22969650 http://dx.doi.org/10.1107/S1600536812036227 Text en © Sharma et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Sharma, Garima
Kumar, S. Vasanth
Wahab, Habibah A.
Rosli, Mohd Mustaqim
Fun, Hoong-Kun
(3′R)-3′-Benzyl-2′,3′-dihydro-1H-spiro­[indole-3,1′-naphtho­[2,3-c]pyrrole]-2,4′,9′-trione
title (3′R)-3′-Benzyl-2′,3′-dihydro-1H-spiro­[indole-3,1′-naphtho­[2,3-c]pyrrole]-2,4′,9′-trione
title_full (3′R)-3′-Benzyl-2′,3′-dihydro-1H-spiro­[indole-3,1′-naphtho­[2,3-c]pyrrole]-2,4′,9′-trione
title_fullStr (3′R)-3′-Benzyl-2′,3′-dihydro-1H-spiro­[indole-3,1′-naphtho­[2,3-c]pyrrole]-2,4′,9′-trione
title_full_unstemmed (3′R)-3′-Benzyl-2′,3′-dihydro-1H-spiro­[indole-3,1′-naphtho­[2,3-c]pyrrole]-2,4′,9′-trione
title_short (3′R)-3′-Benzyl-2′,3′-dihydro-1H-spiro­[indole-3,1′-naphtho­[2,3-c]pyrrole]-2,4′,9′-trione
title_sort (3′r)-3′-benzyl-2′,3′-dihydro-1h-spiro­[indole-3,1′-naphtho­[2,3-c]pyrrole]-2,4′,9′-trione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3435804/
https://www.ncbi.nlm.nih.gov/pubmed/22969650
http://dx.doi.org/10.1107/S1600536812036227
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