(E)-4-Meth­oxy-N′-[(pyridin-4-yl)methyl­idene]benzohydrazide monohydrate

In the title compound, C(14)H(13)N(3)O(2)·H(2)O, the azomethine double bond adopts an E conformation and the N—N=C—C torsion angle is 178.37 (19)°. The dihedral angle between the benzene and pyridine rings is 5.58 (12)° and the C atom of the meth­oxy group is roughly coplanar with its attached ring...

Descripción completa

Detalles Bibliográficos
Autores principales: Taha, Muhammad, Naz, Humera, Rahman, Aqilah Abd, Ismail, Nor Hadiani, Sammer, Yousuf
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3435810/
https://www.ncbi.nlm.nih.gov/pubmed/22969656
http://dx.doi.org/10.1107/S1600536812034988
_version_ 1782242592651476992
author Taha, Muhammad
Naz, Humera
Rahman, Aqilah Abd
Ismail, Nor Hadiani
Sammer, Yousuf
author_facet Taha, Muhammad
Naz, Humera
Rahman, Aqilah Abd
Ismail, Nor Hadiani
Sammer, Yousuf
author_sort Taha, Muhammad
collection PubMed
description In the title compound, C(14)H(13)N(3)O(2)·H(2)O, the azomethine double bond adopts an E conformation and the N—N=C—C torsion angle is 178.37 (19)°. The dihedral angle between the benzene and pyridine rings is 5.58 (12)° and the C atom of the meth­oxy group is roughly coplanar with its attached ring [deviation = 0.157 (3) Å]. In the crystal, the components are linked by O—H⋯O, O—H⋯N, N—H⋯O and C—H⋯O hydrogen bonds, forming (001) sheets. The water O atom accepts one N—H⋯O and two C—H⋯O inter­actions from the adjacent organic mol­ecule.
format Online
Article
Text
id pubmed-3435810
institution National Center for Biotechnology Information
language English
publishDate 2012
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-34358102012-09-11 (E)-4-Meth­oxy-N′-[(pyridin-4-yl)methyl­idene]benzohydrazide monohydrate Taha, Muhammad Naz, Humera Rahman, Aqilah Abd Ismail, Nor Hadiani Sammer, Yousuf Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(14)H(13)N(3)O(2)·H(2)O, the azomethine double bond adopts an E conformation and the N—N=C—C torsion angle is 178.37 (19)°. The dihedral angle between the benzene and pyridine rings is 5.58 (12)° and the C atom of the meth­oxy group is roughly coplanar with its attached ring [deviation = 0.157 (3) Å]. In the crystal, the components are linked by O—H⋯O, O—H⋯N, N—H⋯O and C—H⋯O hydrogen bonds, forming (001) sheets. The water O atom accepts one N—H⋯O and two C—H⋯O inter­actions from the adjacent organic mol­ecule. International Union of Crystallography 2012-08-25 /pmc/articles/PMC3435810/ /pubmed/22969656 http://dx.doi.org/10.1107/S1600536812034988 Text en © Taha et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Taha, Muhammad
Naz, Humera
Rahman, Aqilah Abd
Ismail, Nor Hadiani
Sammer, Yousuf
(E)-4-Meth­oxy-N′-[(pyridin-4-yl)methyl­idene]benzohydrazide monohydrate
title (E)-4-Meth­oxy-N′-[(pyridin-4-yl)methyl­idene]benzohydrazide monohydrate
title_full (E)-4-Meth­oxy-N′-[(pyridin-4-yl)methyl­idene]benzohydrazide monohydrate
title_fullStr (E)-4-Meth­oxy-N′-[(pyridin-4-yl)methyl­idene]benzohydrazide monohydrate
title_full_unstemmed (E)-4-Meth­oxy-N′-[(pyridin-4-yl)methyl­idene]benzohydrazide monohydrate
title_short (E)-4-Meth­oxy-N′-[(pyridin-4-yl)methyl­idene]benzohydrazide monohydrate
title_sort (e)-4-meth­oxy-n′-[(pyridin-4-yl)methyl­idene]benzohydrazide monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3435810/
https://www.ncbi.nlm.nih.gov/pubmed/22969656
http://dx.doi.org/10.1107/S1600536812034988
work_keys_str_mv AT tahamuhammad e4methoxynpyridin4ylmethylidenebenzohydrazidemonohydrate
AT nazhumera e4methoxynpyridin4ylmethylidenebenzohydrazidemonohydrate
AT rahmanaqilahabd e4methoxynpyridin4ylmethylidenebenzohydrazidemonohydrate
AT ismailnorhadiani e4methoxynpyridin4ylmethylidenebenzohydrazidemonohydrate
AT sammeryousuf e4methoxynpyridin4ylmethylidenebenzohydrazidemonohydrate

Ejemplares similares