Bis(dicyclo­hexyl­aminium) 2-carb­oxy­methyl-2-hy­droxy­succinate ethanol monosolvate

In the title compound, 2C(12)H(24)N(+)·C(6)H(6)O(7) (2−)·C(2)H(6)O, the cyclo­hexane rings of the cations adopt chair conformations. In the anion, intra­molecular O—H⋯O hydrogen bonds occur. In the crystal, the cations link with the anions via N—H⋯O hydrogen bonds. Weak C—H⋯O hydrogen bonds are also...

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Autores principales: Foroughian, Mahsa, Notash, Behrouz, Shafiee, Abbas, Aghabozorg, Hossein, Foroumadi, Alireza
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3435822/
https://www.ncbi.nlm.nih.gov/pubmed/22969668
http://dx.doi.org/10.1107/S1600536812035684
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author Foroughian, Mahsa
Notash, Behrouz
Shafiee, Abbas
Aghabozorg, Hossein
Foroumadi, Alireza
author_facet Foroughian, Mahsa
Notash, Behrouz
Shafiee, Abbas
Aghabozorg, Hossein
Foroumadi, Alireza
author_sort Foroughian, Mahsa
collection PubMed
description In the title compound, 2C(12)H(24)N(+)·C(6)H(6)O(7) (2−)·C(2)H(6)O, the cyclo­hexane rings of the cations adopt chair conformations. In the anion, intra­molecular O—H⋯O hydrogen bonds occur. In the crystal, the cations link with the anions via N—H⋯O hydrogen bonds. Weak C—H⋯O hydrogen bonds are also observed. The hy­droxy group of the ethanol solvent mol­ecule is disordered over two sets of sites with an occupancy ratio of 0.766 (5):0.234 (5).
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spelling pubmed-34358222012-09-11 Bis(dicyclo­hexyl­aminium) 2-carb­oxy­methyl-2-hy­droxy­succinate ethanol monosolvate Foroughian, Mahsa Notash, Behrouz Shafiee, Abbas Aghabozorg, Hossein Foroumadi, Alireza Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, 2C(12)H(24)N(+)·C(6)H(6)O(7) (2−)·C(2)H(6)O, the cyclo­hexane rings of the cations adopt chair conformations. In the anion, intra­molecular O—H⋯O hydrogen bonds occur. In the crystal, the cations link with the anions via N—H⋯O hydrogen bonds. Weak C—H⋯O hydrogen bonds are also observed. The hy­droxy group of the ethanol solvent mol­ecule is disordered over two sets of sites with an occupancy ratio of 0.766 (5):0.234 (5). International Union of Crystallography 2012-08-25 /pmc/articles/PMC3435822/ /pubmed/22969668 http://dx.doi.org/10.1107/S1600536812035684 Text en © Foroughian et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Foroughian, Mahsa
Notash, Behrouz
Shafiee, Abbas
Aghabozorg, Hossein
Foroumadi, Alireza
Bis(dicyclo­hexyl­aminium) 2-carb­oxy­methyl-2-hy­droxy­succinate ethanol monosolvate
title Bis(dicyclo­hexyl­aminium) 2-carb­oxy­methyl-2-hy­droxy­succinate ethanol monosolvate
title_full Bis(dicyclo­hexyl­aminium) 2-carb­oxy­methyl-2-hy­droxy­succinate ethanol monosolvate
title_fullStr Bis(dicyclo­hexyl­aminium) 2-carb­oxy­methyl-2-hy­droxy­succinate ethanol monosolvate
title_full_unstemmed Bis(dicyclo­hexyl­aminium) 2-carb­oxy­methyl-2-hy­droxy­succinate ethanol monosolvate
title_short Bis(dicyclo­hexyl­aminium) 2-carb­oxy­methyl-2-hy­droxy­succinate ethanol monosolvate
title_sort bis(dicyclo­hexyl­aminium) 2-carb­oxy­methyl-2-hy­droxy­succinate ethanol monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3435822/
https://www.ncbi.nlm.nih.gov/pubmed/22969668
http://dx.doi.org/10.1107/S1600536812035684
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