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Synthesis of size-controlled monodisperse Pd nanoparticles via a non-aqueous seed-mediated growth

We demonstrated that stepwise seed-mediated growth could be extended in non-aqueous solution (solvothermal synthesis) and improved as an effective method for controlling the uniform size of palladium nanoparticles (Pd NPs) in a wide range. The monodisperse Pd NPs with the size of about 5 nm were syn...

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Detalles Bibliográficos
Autores principales: Zhang, Lei, Wang, Lin, Jiang, Zhiyuan, Xie, Zhaoxiong
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Springer 2012
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3462717/
https://www.ncbi.nlm.nih.gov/pubmed/22713177
http://dx.doi.org/10.1186/1556-276X-7-312
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author Zhang, Lei
Wang, Lin
Jiang, Zhiyuan
Xie, Zhaoxiong
author_facet Zhang, Lei
Wang, Lin
Jiang, Zhiyuan
Xie, Zhaoxiong
author_sort Zhang, Lei
collection PubMed
description We demonstrated that stepwise seed-mediated growth could be extended in non-aqueous solution (solvothermal synthesis) and improved as an effective method for controlling the uniform size of palladium nanoparticles (Pd NPs) in a wide range. The monodisperse Pd NPs with the size of about 5 nm were synthesized by simply reducing Pd(acac)(2) with formaldehyde in different organic amine solvents. By an improved stepwise seed-mediated synthesis, the size of the monodisperse Pd NPs can be precisely controlled from approximately 5 to 10 nm. The as-prepared Pd NPs could self assemble to well-shaped superlattice crystal without size selection process.
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spelling pubmed-34627172012-10-03 Synthesis of size-controlled monodisperse Pd nanoparticles via a non-aqueous seed-mediated growth Zhang, Lei Wang, Lin Jiang, Zhiyuan Xie, Zhaoxiong Nanoscale Res Lett Nano Express We demonstrated that stepwise seed-mediated growth could be extended in non-aqueous solution (solvothermal synthesis) and improved as an effective method for controlling the uniform size of palladium nanoparticles (Pd NPs) in a wide range. The monodisperse Pd NPs with the size of about 5 nm were synthesized by simply reducing Pd(acac)(2) with formaldehyde in different organic amine solvents. By an improved stepwise seed-mediated synthesis, the size of the monodisperse Pd NPs can be precisely controlled from approximately 5 to 10 nm. The as-prepared Pd NPs could self assemble to well-shaped superlattice crystal without size selection process. Springer 2012-06-19 /pmc/articles/PMC3462717/ /pubmed/22713177 http://dx.doi.org/10.1186/1556-276X-7-312 Text en Copyright ©2012 Zhang et al.; licensee Springer. http://creativecommons.org/licenses/by/2.0 This is an Open Access article distributed under the terms of the Creative Commons Attribution License (http://creativecommons.org/licenses/by/2.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
spellingShingle Nano Express
Zhang, Lei
Wang, Lin
Jiang, Zhiyuan
Xie, Zhaoxiong
Synthesis of size-controlled monodisperse Pd nanoparticles via a non-aqueous seed-mediated growth
title Synthesis of size-controlled monodisperse Pd nanoparticles via a non-aqueous seed-mediated growth
title_full Synthesis of size-controlled monodisperse Pd nanoparticles via a non-aqueous seed-mediated growth
title_fullStr Synthesis of size-controlled monodisperse Pd nanoparticles via a non-aqueous seed-mediated growth
title_full_unstemmed Synthesis of size-controlled monodisperse Pd nanoparticles via a non-aqueous seed-mediated growth
title_short Synthesis of size-controlled monodisperse Pd nanoparticles via a non-aqueous seed-mediated growth
title_sort synthesis of size-controlled monodisperse pd nanoparticles via a non-aqueous seed-mediated growth
topic Nano Express
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3462717/
https://www.ncbi.nlm.nih.gov/pubmed/22713177
http://dx.doi.org/10.1186/1556-276X-7-312
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