(E)-4-Meth­oxy-N′-(3,4,5-trihy­droxy­benzyl­idene)benzohydrazide methanol monosolvate

The title compound, C(15)H(14)N(2)O(5)·CH(3)OH, displays an E conformation about the azomethine double bond [C=N = 1.277 (2) Å] and the benzene rings are inclined to one another by 18.28 (9)°. An intra­molecular O—H⋯O hydrogen bond occurs between the para-OH group and one of the meta-O atoms of the...

Descripción completa

Detalles Bibliográficos
Autores principales: Taha, Muhammad, Naz, Humera, Rahman, Aqilah Abd, Ismail, Nor Hadiani, Yousuf, Sammer
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3470206/
https://www.ncbi.nlm.nih.gov/pubmed/23125650
http://dx.doi.org/10.1107/S1600536812036550
_version_ 1782246219684249600
author Taha, Muhammad
Naz, Humera
Rahman, Aqilah Abd
Ismail, Nor Hadiani
Yousuf, Sammer
author_facet Taha, Muhammad
Naz, Humera
Rahman, Aqilah Abd
Ismail, Nor Hadiani
Yousuf, Sammer
author_sort Taha, Muhammad
collection PubMed
description The title compound, C(15)H(14)N(2)O(5)·CH(3)OH, displays an E conformation about the azomethine double bond [C=N = 1.277 (2) Å] and the benzene rings are inclined to one another by 18.28 (9)°. An intra­molecular O—H⋯O hydrogen bond occurs between the para-OH group and one of the meta-O atoms of the 3,4,5-trihy­droxy­benzyl­idene group. In the crystal, the components are linked into a three dimensional network by O—H⋯O, O—H⋯N and C—H⋯O hydrogen bonds.
format Online
Article
Text
id pubmed-3470206
institution National Center for Biotechnology Information
language English
publishDate 2012
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-34702062012-11-02 (E)-4-Meth­oxy-N′-(3,4,5-trihy­droxy­benzyl­idene)benzohydrazide methanol monosolvate Taha, Muhammad Naz, Humera Rahman, Aqilah Abd Ismail, Nor Hadiani Yousuf, Sammer Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(15)H(14)N(2)O(5)·CH(3)OH, displays an E conformation about the azomethine double bond [C=N = 1.277 (2) Å] and the benzene rings are inclined to one another by 18.28 (9)°. An intra­molecular O—H⋯O hydrogen bond occurs between the para-OH group and one of the meta-O atoms of the 3,4,5-trihy­droxy­benzyl­idene group. In the crystal, the components are linked into a three dimensional network by O—H⋯O, O—H⋯N and C—H⋯O hydrogen bonds. International Union of Crystallography 2012-09-05 /pmc/articles/PMC3470206/ /pubmed/23125650 http://dx.doi.org/10.1107/S1600536812036550 Text en © Taha et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Taha, Muhammad
Naz, Humera
Rahman, Aqilah Abd
Ismail, Nor Hadiani
Yousuf, Sammer
(E)-4-Meth­oxy-N′-(3,4,5-trihy­droxy­benzyl­idene)benzohydrazide methanol monosolvate
title (E)-4-Meth­oxy-N′-(3,4,5-trihy­droxy­benzyl­idene)benzohydrazide methanol monosolvate
title_full (E)-4-Meth­oxy-N′-(3,4,5-trihy­droxy­benzyl­idene)benzohydrazide methanol monosolvate
title_fullStr (E)-4-Meth­oxy-N′-(3,4,5-trihy­droxy­benzyl­idene)benzohydrazide methanol monosolvate
title_full_unstemmed (E)-4-Meth­oxy-N′-(3,4,5-trihy­droxy­benzyl­idene)benzohydrazide methanol monosolvate
title_short (E)-4-Meth­oxy-N′-(3,4,5-trihy­droxy­benzyl­idene)benzohydrazide methanol monosolvate
title_sort (e)-4-meth­oxy-n′-(3,4,5-trihy­droxy­benzyl­idene)benzohydrazide methanol monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3470206/
https://www.ncbi.nlm.nih.gov/pubmed/23125650
http://dx.doi.org/10.1107/S1600536812036550
work_keys_str_mv AT tahamuhammad e4methoxyn345trihydroxybenzylidenebenzohydrazidemethanolmonosolvate
AT nazhumera e4methoxyn345trihydroxybenzylidenebenzohydrazidemethanolmonosolvate
AT rahmanaqilahabd e4methoxyn345trihydroxybenzylidenebenzohydrazidemethanolmonosolvate
AT ismailnorhadiani e4methoxyn345trihydroxybenzylidenebenzohydrazidemethanolmonosolvate
AT yousufsammer e4methoxyn345trihydroxybenzylidenebenzohydrazidemethanolmonosolvate

Ejemplares similares