2-Carbamoyl-3,4,5,6-tetra­fluoro­benzoic acid

In the title compound, C(8)H(3)F(4)NO(3), the carb­oxy group lies nearly in the plane of the ring with a C—C—C—O torsion angle of −10.5 (4)°. The carbamoyl group is almost perpendic­ular to the benzene ring [C—C—C—O torsion angle = 82.2 (4) °]. In the crystal, molecules are linked via O—H⋯O and N—H⋯...

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Detalles Bibliográficos
Autores principales: Lu, Tao, Liao, Xiao-Jian, Liang, Yuan-Wei, Xu, Shi-Hai
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3470221/
https://www.ncbi.nlm.nih.gov/pubmed/23125665
http://dx.doi.org/10.1107/S1600536812036549
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author Lu, Tao
Liao, Xiao-Jian
Liang, Yuan-Wei
Xu, Shi-Hai
author_facet Lu, Tao
Liao, Xiao-Jian
Liang, Yuan-Wei
Xu, Shi-Hai
author_sort Lu, Tao
collection PubMed
description In the title compound, C(8)H(3)F(4)NO(3), the carb­oxy group lies nearly in the plane of the ring with a C—C—C—O torsion angle of −10.5 (4)°. The carbamoyl group is almost perpendic­ular to the benzene ring [C—C—C—O torsion angle = 82.2 (4) °]. In the crystal, molecules are linked via O—H⋯O and N—H⋯O hydrogen bonds involving the carbamoyl and carb­oxy groups.
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spelling pubmed-34702212012-11-02 2-Carbamoyl-3,4,5,6-tetra­fluoro­benzoic acid Lu, Tao Liao, Xiao-Jian Liang, Yuan-Wei Xu, Shi-Hai Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(8)H(3)F(4)NO(3), the carb­oxy group lies nearly in the plane of the ring with a C—C—C—O torsion angle of −10.5 (4)°. The carbamoyl group is almost perpendic­ular to the benzene ring [C—C—C—O torsion angle = 82.2 (4) °]. In the crystal, molecules are linked via O—H⋯O and N—H⋯O hydrogen bonds involving the carbamoyl and carb­oxy groups. International Union of Crystallography 2012-09-05 /pmc/articles/PMC3470221/ /pubmed/23125665 http://dx.doi.org/10.1107/S1600536812036549 Text en © Lu et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Lu, Tao
Liao, Xiao-Jian
Liang, Yuan-Wei
Xu, Shi-Hai
2-Carbamoyl-3,4,5,6-tetra­fluoro­benzoic acid
title 2-Carbamoyl-3,4,5,6-tetra­fluoro­benzoic acid
title_full 2-Carbamoyl-3,4,5,6-tetra­fluoro­benzoic acid
title_fullStr 2-Carbamoyl-3,4,5,6-tetra­fluoro­benzoic acid
title_full_unstemmed 2-Carbamoyl-3,4,5,6-tetra­fluoro­benzoic acid
title_short 2-Carbamoyl-3,4,5,6-tetra­fluoro­benzoic acid
title_sort 2-carbamoyl-3,4,5,6-tetra­fluoro­benzoic acid
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3470221/
https://www.ncbi.nlm.nih.gov/pubmed/23125665
http://dx.doi.org/10.1107/S1600536812036549
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