Ethyl 2-benzene­sulfonamido-4-methyl­penta­noate

In the title compound, C(14)H(21)NO(4)S, the O—S—O angle is 120.06 (11)°, with the S atom adopting a distorted tetra­hedral geometry. In the crystal, N—H⋯O hydrogen bonds connect the mol­ecules along the a axis, generating an infinite chain. The disordered C atoms of the isobutyl group were refined...

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Detalles Bibliográficos
Autores principales: Arshad, Muhammad Nadeem, Danish, Muhammad, Tahir, Muhammad Nawaz, Khalid, Savera, Asiri, Abdullah M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3470229/
https://www.ncbi.nlm.nih.gov/pubmed/23125673
http://dx.doi.org/10.1107/S1600536812037658
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author Arshad, Muhammad Nadeem
Danish, Muhammad
Tahir, Muhammad Nawaz
Khalid, Savera
Asiri, Abdullah M.
author_facet Arshad, Muhammad Nadeem
Danish, Muhammad
Tahir, Muhammad Nawaz
Khalid, Savera
Asiri, Abdullah M.
author_sort Arshad, Muhammad Nadeem
collection PubMed
description In the title compound, C(14)H(21)NO(4)S, the O—S—O angle is 120.06 (11)°, with the S atom adopting a distorted tetra­hedral geometry. In the crystal, N—H⋯O hydrogen bonds connect the mol­ecules along the a axis, generating an infinite chain. The disordered C atoms of the isobutyl group were refined with the C—C distances restrained to 1.52 (1) Å and the occupancy ratio refined to 0.504 (3):0.496 (3).
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spelling pubmed-34702292012-11-02 Ethyl 2-benzene­sulfonamido-4-methyl­penta­noate Arshad, Muhammad Nadeem Danish, Muhammad Tahir, Muhammad Nawaz Khalid, Savera Asiri, Abdullah M. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(14)H(21)NO(4)S, the O—S—O angle is 120.06 (11)°, with the S atom adopting a distorted tetra­hedral geometry. In the crystal, N—H⋯O hydrogen bonds connect the mol­ecules along the a axis, generating an infinite chain. The disordered C atoms of the isobutyl group were refined with the C—C distances restrained to 1.52 (1) Å and the occupancy ratio refined to 0.504 (3):0.496 (3). International Union of Crystallography 2012-09-08 /pmc/articles/PMC3470229/ /pubmed/23125673 http://dx.doi.org/10.1107/S1600536812037658 Text en © Arshad et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Arshad, Muhammad Nadeem
Danish, Muhammad
Tahir, Muhammad Nawaz
Khalid, Savera
Asiri, Abdullah M.
Ethyl 2-benzene­sulfonamido-4-methyl­penta­noate
title Ethyl 2-benzene­sulfonamido-4-methyl­penta­noate
title_full Ethyl 2-benzene­sulfonamido-4-methyl­penta­noate
title_fullStr Ethyl 2-benzene­sulfonamido-4-methyl­penta­noate
title_full_unstemmed Ethyl 2-benzene­sulfonamido-4-methyl­penta­noate
title_short Ethyl 2-benzene­sulfonamido-4-methyl­penta­noate
title_sort ethyl 2-benzene­sulfonamido-4-methyl­penta­noate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3470229/
https://www.ncbi.nlm.nih.gov/pubmed/23125673
http://dx.doi.org/10.1107/S1600536812037658
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