Bis(2-methyl-1H-benzimidazol-3-ium) naphthalene-1,5-disulfonate

The asymmetric unit of the title compound, 2C(8)H(9)N(2) (+)·C(10)H(6)O(6)S(2) (2−), contains a 2-methyl­benzimidazolium cation and one half of a naphthalene-1,5-disulfonate anion. The formula unit is generated by an inversion center. In the crystal, N—H⋯O hydrogen bonds link the components into cha...

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Autores principales: Wei, Shuai-Shuai, Jin, Shou-Wen, Dong, Qiong, Cao, Xin-Chao, Yu, Ze-Yun
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3470333/
https://www.ncbi.nlm.nih.gov/pubmed/23125746
http://dx.doi.org/10.1107/S1600536812039396
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author Wei, Shuai-Shuai
Jin, Shou-Wen
Dong, Qiong
Cao, Xin-Chao
Yu, Ze-Yun
author_facet Wei, Shuai-Shuai
Jin, Shou-Wen
Dong, Qiong
Cao, Xin-Chao
Yu, Ze-Yun
author_sort Wei, Shuai-Shuai
collection PubMed
description The asymmetric unit of the title compound, 2C(8)H(9)N(2) (+)·C(10)H(6)O(6)S(2) (2−), contains a 2-methyl­benzimidazolium cation and one half of a naphthalene-1,5-disulfonate anion. The formula unit is generated by an inversion center. In the crystal, N—H⋯O hydrogen bonds link the components into chains along [001]. In addition, weak C—H⋯O hydrogen bonds and weak C—H⋯π inter­actions are observed. The methyl H atoms were refined as disordered over two sets of sites with equal occupancy.
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spelling pubmed-34703332012-11-02 Bis(2-methyl-1H-benzimidazol-3-ium) naphthalene-1,5-disulfonate Wei, Shuai-Shuai Jin, Shou-Wen Dong, Qiong Cao, Xin-Chao Yu, Ze-Yun Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, 2C(8)H(9)N(2) (+)·C(10)H(6)O(6)S(2) (2−), contains a 2-methyl­benzimidazolium cation and one half of a naphthalene-1,5-disulfonate anion. The formula unit is generated by an inversion center. In the crystal, N—H⋯O hydrogen bonds link the components into chains along [001]. In addition, weak C—H⋯O hydrogen bonds and weak C—H⋯π inter­actions are observed. The methyl H atoms were refined as disordered over two sets of sites with equal occupancy. International Union of Crystallography 2012-09-22 /pmc/articles/PMC3470333/ /pubmed/23125746 http://dx.doi.org/10.1107/S1600536812039396 Text en © Wei et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wei, Shuai-Shuai
Jin, Shou-Wen
Dong, Qiong
Cao, Xin-Chao
Yu, Ze-Yun
Bis(2-methyl-1H-benzimidazol-3-ium) naphthalene-1,5-disulfonate
title Bis(2-methyl-1H-benzimidazol-3-ium) naphthalene-1,5-disulfonate
title_full Bis(2-methyl-1H-benzimidazol-3-ium) naphthalene-1,5-disulfonate
title_fullStr Bis(2-methyl-1H-benzimidazol-3-ium) naphthalene-1,5-disulfonate
title_full_unstemmed Bis(2-methyl-1H-benzimidazol-3-ium) naphthalene-1,5-disulfonate
title_short Bis(2-methyl-1H-benzimidazol-3-ium) naphthalene-1,5-disulfonate
title_sort bis(2-methyl-1h-benzimidazol-3-ium) naphthalene-1,5-disulfonate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3470333/
https://www.ncbi.nlm.nih.gov/pubmed/23125746
http://dx.doi.org/10.1107/S1600536812039396
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