Cargando…
A co-crystal of 3-(3,5-dinitrobenzoyl)-1,1-dimethylthiourea and N,N-dimethyl-3,5-dinitrobenzamide
In the title compound, C(10)H(10)N(4)O(5)S·C(9)H(9)N(3)O(5), the amide groups of 3-(3,5-dinitro-benzoyl)-1,1-dimethyl-thiourea and N,N-dimethyl-3,5-dinitro-benzamide molecules are oriented at dihedral angles of 39.13 (8) and 55.97 (11)°, respectively, to the attached benzene rings. In the crystal...
| Autores principales: | , , , , |
|---|---|
| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2012
|
| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3515214/ https://www.ncbi.nlm.nih.gov/pubmed/23284434 http://dx.doi.org/10.1107/S1600536812041864 |
| _version_ | 1782252135340048384 |
|---|---|
| author | Saeed, Sohail Rashid, Naghmana Butcher, Ray J. Öztürk Yildirim, Sema Hussain, Rizwan |
| author_facet | Saeed, Sohail Rashid, Naghmana Butcher, Ray J. Öztürk Yildirim, Sema Hussain, Rizwan |
| author_sort | Saeed, Sohail |
| collection | PubMed |
| description | In the title compound, C(10)H(10)N(4)O(5)S·C(9)H(9)N(3)O(5), the amide groups of 3-(3,5-dinitro-benzoyl)-1,1-dimethyl-thiourea and N,N-dimethyl-3,5-dinitro-benzamide molecules are oriented at dihedral angles of 39.13 (8) and 55.97 (11)°, respectively, to the attached benzene rings. In the crystal, the two molecules are linked by an N—H⋯O hydrogen bond. Weak C—H⋯O link the molecules into a sheet parallel to the bc plane. C—H⋯S interactions also occur. |
| format | Online Article Text |
| id | pubmed-3515214 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2012 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-35152142013-01-02 A co-crystal of 3-(3,5-dinitrobenzoyl)-1,1-dimethylthiourea and N,N-dimethyl-3,5-dinitrobenzamide Saeed, Sohail Rashid, Naghmana Butcher, Ray J. Öztürk Yildirim, Sema Hussain, Rizwan Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(10)H(10)N(4)O(5)S·C(9)H(9)N(3)O(5), the amide groups of 3-(3,5-dinitro-benzoyl)-1,1-dimethyl-thiourea and N,N-dimethyl-3,5-dinitro-benzamide molecules are oriented at dihedral angles of 39.13 (8) and 55.97 (11)°, respectively, to the attached benzene rings. In the crystal, the two molecules are linked by an N—H⋯O hydrogen bond. Weak C—H⋯O link the molecules into a sheet parallel to the bc plane. C—H⋯S interactions also occur. International Union of Crystallography 2012-10-13 /pmc/articles/PMC3515214/ /pubmed/23284434 http://dx.doi.org/10.1107/S1600536812041864 Text en © Saeed et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Organic Papers Saeed, Sohail Rashid, Naghmana Butcher, Ray J. Öztürk Yildirim, Sema Hussain, Rizwan A co-crystal of 3-(3,5-dinitrobenzoyl)-1,1-dimethylthiourea and N,N-dimethyl-3,5-dinitrobenzamide |
| title | A co-crystal of 3-(3,5-dinitrobenzoyl)-1,1-dimethylthiourea and N,N-dimethyl-3,5-dinitrobenzamide |
| title_full | A co-crystal of 3-(3,5-dinitrobenzoyl)-1,1-dimethylthiourea and N,N-dimethyl-3,5-dinitrobenzamide |
| title_fullStr | A co-crystal of 3-(3,5-dinitrobenzoyl)-1,1-dimethylthiourea and N,N-dimethyl-3,5-dinitrobenzamide |
| title_full_unstemmed | A co-crystal of 3-(3,5-dinitrobenzoyl)-1,1-dimethylthiourea and N,N-dimethyl-3,5-dinitrobenzamide |
| title_short | A co-crystal of 3-(3,5-dinitrobenzoyl)-1,1-dimethylthiourea and N,N-dimethyl-3,5-dinitrobenzamide |
| title_sort | co-crystal of 3-(3,5-dinitrobenzoyl)-1,1-dimethylthiourea and n,n-dimethyl-3,5-dinitrobenzamide |
| topic | Organic Papers |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3515214/ https://www.ncbi.nlm.nih.gov/pubmed/23284434 http://dx.doi.org/10.1107/S1600536812041864 |
| work_keys_str_mv | AT saeedsohail acocrystalof335dinitrobenzoyl11dimethylthioureaandnndimethyl35dinitrobenzamide AT rashidnaghmana acocrystalof335dinitrobenzoyl11dimethylthioureaandnndimethyl35dinitrobenzamide AT butcherrayj acocrystalof335dinitrobenzoyl11dimethylthioureaandnndimethyl35dinitrobenzamide AT ozturkyildirimsema acocrystalof335dinitrobenzoyl11dimethylthioureaandnndimethyl35dinitrobenzamide AT hussainrizwan acocrystalof335dinitrobenzoyl11dimethylthioureaandnndimethyl35dinitrobenzamide AT saeedsohail cocrystalof335dinitrobenzoyl11dimethylthioureaandnndimethyl35dinitrobenzamide AT rashidnaghmana cocrystalof335dinitrobenzoyl11dimethylthioureaandnndimethyl35dinitrobenzamide AT butcherrayj cocrystalof335dinitrobenzoyl11dimethylthioureaandnndimethyl35dinitrobenzamide AT ozturkyildirimsema cocrystalof335dinitrobenzoyl11dimethylthioureaandnndimethyl35dinitrobenzamide AT hussainrizwan cocrystalof335dinitrobenzoyl11dimethylthioureaandnndimethyl35dinitrobenzamide |