5-[(Z)-2,3-Dimeth­oxy­benzyl­idene]-1,2,4-triazolo[3,2-b][1,3]thia­zol-6(5H)-one

The title compound, C(13)H(11)N(3)O(3)S, was synthesized from 1H-1,2,4-triazole-5-thiol in a one pot reaction. The fused thia­zolo[3,2-b][1,2,4]triazole system is essentially coplanar with the benzene ring: they enclose an inter­planar angle of 1.37 (13)°. The olefinic double bond is in a Z conforma...

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Detalles Bibliográficos
Autores principales: Guo, Lu, Lin, Gao-Tong, Wang, Jia, Ni, Li, Ge, Ren-Shan
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3515241/
https://www.ncbi.nlm.nih.gov/pubmed/23284461
http://dx.doi.org/10.1107/S1600536812042559
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author Guo, Lu
Lin, Gao-Tong
Wang, Jia
Ni, Li
Ge, Ren-Shan
author_facet Guo, Lu
Lin, Gao-Tong
Wang, Jia
Ni, Li
Ge, Ren-Shan
author_sort Guo, Lu
collection PubMed
description The title compound, C(13)H(11)N(3)O(3)S, was synthesized from 1H-1,2,4-triazole-5-thiol in a one pot reaction. The fused thia­zolo[3,2-b][1,2,4]triazole system is essentially coplanar with the benzene ring: they enclose an inter­planar angle of 1.37 (13)°. The olefinic double bond is in a Z conformation. In the crystal, C—H⋯N hydrogen bonds link the mol­ecules into double layers parallel to the ab plane.
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spelling pubmed-35152412013-01-02 5-[(Z)-2,3-Dimeth­oxy­benzyl­idene]-1,2,4-triazolo[3,2-b][1,3]thia­zol-6(5H)-one Guo, Lu Lin, Gao-Tong Wang, Jia Ni, Li Ge, Ren-Shan Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(13)H(11)N(3)O(3)S, was synthesized from 1H-1,2,4-triazole-5-thiol in a one pot reaction. The fused thia­zolo[3,2-b][1,2,4]triazole system is essentially coplanar with the benzene ring: they enclose an inter­planar angle of 1.37 (13)°. The olefinic double bond is in a Z conformation. In the crystal, C—H⋯N hydrogen bonds link the mol­ecules into double layers parallel to the ab plane. International Union of Crystallography 2012-10-20 /pmc/articles/PMC3515241/ /pubmed/23284461 http://dx.doi.org/10.1107/S1600536812042559 Text en © Guo et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Guo, Lu
Lin, Gao-Tong
Wang, Jia
Ni, Li
Ge, Ren-Shan
5-[(Z)-2,3-Dimeth­oxy­benzyl­idene]-1,2,4-triazolo[3,2-b][1,3]thia­zol-6(5H)-one
title 5-[(Z)-2,3-Dimeth­oxy­benzyl­idene]-1,2,4-triazolo[3,2-b][1,3]thia­zol-6(5H)-one
title_full 5-[(Z)-2,3-Dimeth­oxy­benzyl­idene]-1,2,4-triazolo[3,2-b][1,3]thia­zol-6(5H)-one
title_fullStr 5-[(Z)-2,3-Dimeth­oxy­benzyl­idene]-1,2,4-triazolo[3,2-b][1,3]thia­zol-6(5H)-one
title_full_unstemmed 5-[(Z)-2,3-Dimeth­oxy­benzyl­idene]-1,2,4-triazolo[3,2-b][1,3]thia­zol-6(5H)-one
title_short 5-[(Z)-2,3-Dimeth­oxy­benzyl­idene]-1,2,4-triazolo[3,2-b][1,3]thia­zol-6(5H)-one
title_sort 5-[(z)-2,3-dimeth­oxy­benzyl­idene]-1,2,4-triazolo[3,2-b][1,3]thia­zol-6(5h)-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3515241/
https://www.ncbi.nlm.nih.gov/pubmed/23284461
http://dx.doi.org/10.1107/S1600536812042559
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