N,N-Bis(2-hy­droxy­eth­yl)-4-methyl­benzene­sulfonamide

In the title compound C(11)H(17)NO(4)S, an intra­molecular O—H⋯O hydrogen bond forms an S(8) ring and determines the conformation of the bis­(2-hy­droxy­eth­yl) segment of the mol­ecule, holding the two CH(2)CH(2)OH groups close to coplanar (r.m.s. deviation = 0.185 Å). In the crystal, O—H⋯O hydroge...

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Autores principales: Mushtaq, Nafeesa, Khan, Islam Ullah, Yar, Muhammad, Afzal, Sadia, Simpson, Jim
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3515243/
https://www.ncbi.nlm.nih.gov/pubmed/23284463
http://dx.doi.org/10.1107/S1600536812041682
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author Mushtaq, Nafeesa
Khan, Islam Ullah
Yar, Muhammad
Afzal, Sadia
Simpson, Jim
author_facet Mushtaq, Nafeesa
Khan, Islam Ullah
Yar, Muhammad
Afzal, Sadia
Simpson, Jim
author_sort Mushtaq, Nafeesa
collection PubMed
description In the title compound C(11)H(17)NO(4)S, an intra­molecular O—H⋯O hydrogen bond forms an S(8) ring and determines the conformation of the bis­(2-hy­droxy­eth­yl) segment of the mol­ecule, holding the two CH(2)CH(2)OH groups close to coplanar (r.m.s. deviation = 0.185 Å). In the crystal, O—H⋯O hydrogen bonds link the mol­ecules into zigzag chains along the b axis. Weaker additional C—H⋯O and C—H⋯π contacts generate a three dimensional network, with mol­ecules stacked along the b-axis direction.
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spelling pubmed-35152432013-01-02 N,N-Bis(2-hy­droxy­eth­yl)-4-methyl­benzene­sulfonamide Mushtaq, Nafeesa Khan, Islam Ullah Yar, Muhammad Afzal, Sadia Simpson, Jim Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound C(11)H(17)NO(4)S, an intra­molecular O—H⋯O hydrogen bond forms an S(8) ring and determines the conformation of the bis­(2-hy­droxy­eth­yl) segment of the mol­ecule, holding the two CH(2)CH(2)OH groups close to coplanar (r.m.s. deviation = 0.185 Å). In the crystal, O—H⋯O hydrogen bonds link the mol­ecules into zigzag chains along the b axis. Weaker additional C—H⋯O and C—H⋯π contacts generate a three dimensional network, with mol­ecules stacked along the b-axis direction. International Union of Crystallography 2012-10-20 /pmc/articles/PMC3515243/ /pubmed/23284463 http://dx.doi.org/10.1107/S1600536812041682 Text en © Mushtaq et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Mushtaq, Nafeesa
Khan, Islam Ullah
Yar, Muhammad
Afzal, Sadia
Simpson, Jim
N,N-Bis(2-hy­droxy­eth­yl)-4-methyl­benzene­sulfonamide
title N,N-Bis(2-hy­droxy­eth­yl)-4-methyl­benzene­sulfonamide
title_full N,N-Bis(2-hy­droxy­eth­yl)-4-methyl­benzene­sulfonamide
title_fullStr N,N-Bis(2-hy­droxy­eth­yl)-4-methyl­benzene­sulfonamide
title_full_unstemmed N,N-Bis(2-hy­droxy­eth­yl)-4-methyl­benzene­sulfonamide
title_short N,N-Bis(2-hy­droxy­eth­yl)-4-methyl­benzene­sulfonamide
title_sort n,n-bis(2-hy­droxy­eth­yl)-4-methyl­benzene­sulfonamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3515243/
https://www.ncbi.nlm.nih.gov/pubmed/23284463
http://dx.doi.org/10.1107/S1600536812041682
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