(±)-(rel-3R,3′R)-1,1′-Dimethyl-3,3′-bipyrrolidine-2,2′-dithione

The asymmetric unit of the racemic title compound, C(10)H(16)N(2)S(2), a C (2)-symmetric bis­(thiol­actam), contains one half-mol­ecule, the complete mol­ecule being generated by a twofold axis symmetry operation. The five-membered ring is nearly planar, with a maximum deviation of 0.025 (1) Å. In t...

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Detalles Bibliográficos
Autores principales: Madeley, Lee G., Lemmerer, Andreas, Michael, Joseph P.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3515298/
https://www.ncbi.nlm.nih.gov/pubmed/23284518
http://dx.doi.org/10.1107/S1600536812043498
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author Madeley, Lee G.
Lemmerer, Andreas
Michael, Joseph P.
author_facet Madeley, Lee G.
Lemmerer, Andreas
Michael, Joseph P.
author_sort Madeley, Lee G.
collection PubMed
description The asymmetric unit of the racemic title compound, C(10)H(16)N(2)S(2), a C (2)-symmetric bis­(thiol­actam), contains one half-mol­ecule, the complete mol­ecule being generated by a twofold axis symmetry operation. The five-membered ring is nearly planar, with a maximum deviation of 0.025 (1) Å. In the crystal, the mol­ecules are linked via weak C—H⋯S inter­actions, forming infinite chains along the b-axis direction.
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spelling pubmed-35152982013-01-02 (±)-(rel-3R,3′R)-1,1′-Dimethyl-3,3′-bipyrrolidine-2,2′-dithione Madeley, Lee G. Lemmerer, Andreas Michael, Joseph P. Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the racemic title compound, C(10)H(16)N(2)S(2), a C (2)-symmetric bis­(thiol­actam), contains one half-mol­ecule, the complete mol­ecule being generated by a twofold axis symmetry operation. The five-membered ring is nearly planar, with a maximum deviation of 0.025 (1) Å. In the crystal, the mol­ecules are linked via weak C—H⋯S inter­actions, forming infinite chains along the b-axis direction. International Union of Crystallography 2012-10-27 /pmc/articles/PMC3515298/ /pubmed/23284518 http://dx.doi.org/10.1107/S1600536812043498 Text en © Madeley et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Madeley, Lee G.
Lemmerer, Andreas
Michael, Joseph P.
(±)-(rel-3R,3′R)-1,1′-Dimethyl-3,3′-bipyrrolidine-2,2′-dithione
title (±)-(rel-3R,3′R)-1,1′-Dimethyl-3,3′-bipyrrolidine-2,2′-dithione
title_full (±)-(rel-3R,3′R)-1,1′-Dimethyl-3,3′-bipyrrolidine-2,2′-dithione
title_fullStr (±)-(rel-3R,3′R)-1,1′-Dimethyl-3,3′-bipyrrolidine-2,2′-dithione
title_full_unstemmed (±)-(rel-3R,3′R)-1,1′-Dimethyl-3,3′-bipyrrolidine-2,2′-dithione
title_short (±)-(rel-3R,3′R)-1,1′-Dimethyl-3,3′-bipyrrolidine-2,2′-dithione
title_sort (±)-(rel-3r,3′r)-1,1′-dimethyl-3,3′-bipyrrolidine-2,2′-dithione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3515298/
https://www.ncbi.nlm.nih.gov/pubmed/23284518
http://dx.doi.org/10.1107/S1600536812043498
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