2-Chloro-N-[1-(4-chloro­phen­yl)-3-cyano-1H-pyrazol-5-yl]acetamide

The title compound, C(12)H(8)Cl(2)N(4)O, was synthesized by the reaction of 5-amino-1-(4-chloro­phen­yl)-1H-pyrazole-3-carbonitrile and 2-chloro­acetyl chloride. The dihedral angle between the pyrazole and benzene rings is 30.7 (3)°. In the crystal structure, strong N—H⋯O hydrogen bonds link the mol...

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Detalles Bibliográficos
Autores principales: Mu, Hai-ping, Yang, Yang, Jiang, Qiang-hua, Fu, Xiao-dong, Wan, Rong
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3515326/
https://www.ncbi.nlm.nih.gov/pubmed/23284546
http://dx.doi.org/10.1107/S1600536812043966
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author Mu, Hai-ping
Yang, Yang
Jiang, Qiang-hua
Fu, Xiao-dong
Wan, Rong
author_facet Mu, Hai-ping
Yang, Yang
Jiang, Qiang-hua
Fu, Xiao-dong
Wan, Rong
author_sort Mu, Hai-ping
collection PubMed
description The title compound, C(12)H(8)Cl(2)N(4)O, was synthesized by the reaction of 5-amino-1-(4-chloro­phen­yl)-1H-pyrazole-3-carbonitrile and 2-chloro­acetyl chloride. The dihedral angle between the pyrazole and benzene rings is 30.7 (3)°. In the crystal structure, strong N—H⋯O hydrogen bonds link the mol­ecules into chains along [001]. C—H⋯N hydrogen bonds are also present.
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spelling pubmed-35153262013-01-02 2-Chloro-N-[1-(4-chloro­phen­yl)-3-cyano-1H-pyrazol-5-yl]acetamide Mu, Hai-ping Yang, Yang Jiang, Qiang-hua Fu, Xiao-dong Wan, Rong Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(12)H(8)Cl(2)N(4)O, was synthesized by the reaction of 5-amino-1-(4-chloro­phen­yl)-1H-pyrazole-3-carbonitrile and 2-chloro­acetyl chloride. The dihedral angle between the pyrazole and benzene rings is 30.7 (3)°. In the crystal structure, strong N—H⋯O hydrogen bonds link the mol­ecules into chains along [001]. C—H⋯N hydrogen bonds are also present. International Union of Crystallography 2012-10-31 /pmc/articles/PMC3515326/ /pubmed/23284546 http://dx.doi.org/10.1107/S1600536812043966 Text en © Mu et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Mu, Hai-ping
Yang, Yang
Jiang, Qiang-hua
Fu, Xiao-dong
Wan, Rong
2-Chloro-N-[1-(4-chloro­phen­yl)-3-cyano-1H-pyrazol-5-yl]acetamide
title 2-Chloro-N-[1-(4-chloro­phen­yl)-3-cyano-1H-pyrazol-5-yl]acetamide
title_full 2-Chloro-N-[1-(4-chloro­phen­yl)-3-cyano-1H-pyrazol-5-yl]acetamide
title_fullStr 2-Chloro-N-[1-(4-chloro­phen­yl)-3-cyano-1H-pyrazol-5-yl]acetamide
title_full_unstemmed 2-Chloro-N-[1-(4-chloro­phen­yl)-3-cyano-1H-pyrazol-5-yl]acetamide
title_short 2-Chloro-N-[1-(4-chloro­phen­yl)-3-cyano-1H-pyrazol-5-yl]acetamide
title_sort 2-chloro-n-[1-(4-chloro­phen­yl)-3-cyano-1h-pyrazol-5-yl]acetamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3515326/
https://www.ncbi.nlm.nih.gov/pubmed/23284546
http://dx.doi.org/10.1107/S1600536812043966
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AT jiangqianghua 2chloron14chlorophenyl3cyano1hpyrazol5ylacetamide
AT fuxiaodong 2chloron14chlorophenyl3cyano1hpyrazol5ylacetamide
AT wanrong 2chloron14chlorophenyl3cyano1hpyrazol5ylacetamide

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