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Thermal noise limit for ultra-high vacuum noncontact atomic force microscopy

The noise of the frequency-shift signal Δf in noncontact atomic force microscopy (NC-AFM) consists of cantilever thermal noise, tip–surface-interaction noise and instrumental noise from the detection and signal processing systems. We investigate how the displacement-noise spectral density d(z) at th...

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Autores principales: Lübbe, Jannis, Temmen, Matthias, Rode, Sebastian, Rahe, Philipp, Kühnle, Angelika, Reichling, Michael
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Beilstein-Institut 2013
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3566860/
https://www.ncbi.nlm.nih.gov/pubmed/23400758
http://dx.doi.org/10.3762/bjnano.4.4
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author Lübbe, Jannis
Temmen, Matthias
Rode, Sebastian
Rahe, Philipp
Kühnle, Angelika
Reichling, Michael
author_facet Lübbe, Jannis
Temmen, Matthias
Rode, Sebastian
Rahe, Philipp
Kühnle, Angelika
Reichling, Michael
author_sort Lübbe, Jannis
collection PubMed
description The noise of the frequency-shift signal Δf in noncontact atomic force microscopy (NC-AFM) consists of cantilever thermal noise, tip–surface-interaction noise and instrumental noise from the detection and signal processing systems. We investigate how the displacement-noise spectral density d(z) at the input of the frequency demodulator propagates to the frequency-shift-noise spectral density d(Δ)(f) at the demodulator output in dependence of cantilever properties and settings of the signal processing electronics in the limit of a negligible tip–surface interaction and a measurement under ultrahigh-vacuum conditions. For a quantification of the noise figures, we calibrate the cantilever displacement signal and determine the transfer function of the signal-processing electronics. From the transfer function and the measured d(z), we predict d(Δ)(f) for specific filter settings, a given level of detection-system noise spectral density d(z)(ds) and the cantilever-thermal-noise spectral density d(z)(th). We find an excellent agreement between the calculated and measured values for d(Δ)(f). Furthermore, we demonstrate that thermal noise in d(Δ)(f), defining the ultimate limit in NC-AFM signal detection, can be kept low by a proper choice of the cantilever whereby its Q-factor should be given most attention. A system with a low-noise signal detection and a suitable cantilever, operated with appropriate filter and feedback-loop settings allows room temperature NC-AFM measurements at a low thermal-noise limit with a significant bandwidth.
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spelling pubmed-35668602013-02-11 Thermal noise limit for ultra-high vacuum noncontact atomic force microscopy Lübbe, Jannis Temmen, Matthias Rode, Sebastian Rahe, Philipp Kühnle, Angelika Reichling, Michael Beilstein J Nanotechnol Full Research Paper The noise of the frequency-shift signal Δf in noncontact atomic force microscopy (NC-AFM) consists of cantilever thermal noise, tip–surface-interaction noise and instrumental noise from the detection and signal processing systems. We investigate how the displacement-noise spectral density d(z) at the input of the frequency demodulator propagates to the frequency-shift-noise spectral density d(Δ)(f) at the demodulator output in dependence of cantilever properties and settings of the signal processing electronics in the limit of a negligible tip–surface interaction and a measurement under ultrahigh-vacuum conditions. For a quantification of the noise figures, we calibrate the cantilever displacement signal and determine the transfer function of the signal-processing electronics. From the transfer function and the measured d(z), we predict d(Δ)(f) for specific filter settings, a given level of detection-system noise spectral density d(z)(ds) and the cantilever-thermal-noise spectral density d(z)(th). We find an excellent agreement between the calculated and measured values for d(Δ)(f). Furthermore, we demonstrate that thermal noise in d(Δ)(f), defining the ultimate limit in NC-AFM signal detection, can be kept low by a proper choice of the cantilever whereby its Q-factor should be given most attention. A system with a low-noise signal detection and a suitable cantilever, operated with appropriate filter and feedback-loop settings allows room temperature NC-AFM measurements at a low thermal-noise limit with a significant bandwidth. Beilstein-Institut 2013-01-17 /pmc/articles/PMC3566860/ /pubmed/23400758 http://dx.doi.org/10.3762/bjnano.4.4 Text en Copyright © 2013, Lübbe et al. https://creativecommons.org/licenses/by/2.0https://www.beilstein-journals.org/bjnano/termsThis is an Open Access article under the terms of the Creative Commons Attribution License (https://creativecommons.org/licenses/by/2.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. The license is subject to the Beilstein Journal of Nanotechnology terms and conditions: (https://www.beilstein-journals.org/bjnano/terms)
spellingShingle Full Research Paper
Lübbe, Jannis
Temmen, Matthias
Rode, Sebastian
Rahe, Philipp
Kühnle, Angelika
Reichling, Michael
Thermal noise limit for ultra-high vacuum noncontact atomic force microscopy
title Thermal noise limit for ultra-high vacuum noncontact atomic force microscopy
title_full Thermal noise limit for ultra-high vacuum noncontact atomic force microscopy
title_fullStr Thermal noise limit for ultra-high vacuum noncontact atomic force microscopy
title_full_unstemmed Thermal noise limit for ultra-high vacuum noncontact atomic force microscopy
title_short Thermal noise limit for ultra-high vacuum noncontact atomic force microscopy
title_sort thermal noise limit for ultra-high vacuum noncontact atomic force microscopy
topic Full Research Paper
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3566860/
https://www.ncbi.nlm.nih.gov/pubmed/23400758
http://dx.doi.org/10.3762/bjnano.4.4
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