9-[3-(Dimethyl­amino)­prop­yl]-10,10-dimethyl-9,10-dihydro­anthracen-9-ol

The asymmetric unit of the title compound, C(21)H(27)NO, contains two mol­ecules (A and B). In mol­ecule A, the central ring of the anthrone unit adopts a shallow boat conformation and the dihedral angle between the benzene rings is 18.96 (7)°. In mol­ecule B, the central ring is close to being plan...

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Detalles Bibliográficos
Autores principales: Kaur, Manpreet, Butcher, Ray J., Akkurt, Mehmet, Yathirajan, H. S., Nagaraj, B.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3569237/
https://www.ncbi.nlm.nih.gov/pubmed/23424460
http://dx.doi.org/10.1107/S1600536812050088
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author Kaur, Manpreet
Butcher, Ray J.
Akkurt, Mehmet
Yathirajan, H. S.
Nagaraj, B.
author_facet Kaur, Manpreet
Butcher, Ray J.
Akkurt, Mehmet
Yathirajan, H. S.
Nagaraj, B.
author_sort Kaur, Manpreet
collection PubMed
description The asymmetric unit of the title compound, C(21)H(27)NO, contains two mol­ecules (A and B). In mol­ecule A, the central ring of the anthrone unit adopts a shallow boat conformation and the dihedral angle between the benzene rings is 18.96 (7)°. In mol­ecule B, the central ring is close to being planar (r.m.s. deviation = 0.078 Å) and the dihedral angle between the aromatic rings is 7.82 (7)°. In the crystal, mol­ecules are linked by O—H⋯N hydrogen bonds, forming zigzag C(7) chains of alternating A and B mol­ecules running parallel to [100]. The structure also features weak C—H⋯O and C—H⋯π inter­actions.
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spelling pubmed-35692372013-02-19 9-[3-(Dimethyl­amino)­prop­yl]-10,10-dimethyl-9,10-dihydro­anthracen-9-ol Kaur, Manpreet Butcher, Ray J. Akkurt, Mehmet Yathirajan, H. S. Nagaraj, B. Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(21)H(27)NO, contains two mol­ecules (A and B). In mol­ecule A, the central ring of the anthrone unit adopts a shallow boat conformation and the dihedral angle between the benzene rings is 18.96 (7)°. In mol­ecule B, the central ring is close to being planar (r.m.s. deviation = 0.078 Å) and the dihedral angle between the aromatic rings is 7.82 (7)°. In the crystal, mol­ecules are linked by O—H⋯N hydrogen bonds, forming zigzag C(7) chains of alternating A and B mol­ecules running parallel to [100]. The structure also features weak C—H⋯O and C—H⋯π inter­actions. International Union of Crystallography 2013-01-04 /pmc/articles/PMC3569237/ /pubmed/23424460 http://dx.doi.org/10.1107/S1600536812050088 Text en © Kaur et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Kaur, Manpreet
Butcher, Ray J.
Akkurt, Mehmet
Yathirajan, H. S.
Nagaraj, B.
9-[3-(Dimethyl­amino)­prop­yl]-10,10-dimethyl-9,10-dihydro­anthracen-9-ol
title 9-[3-(Dimethyl­amino)­prop­yl]-10,10-dimethyl-9,10-dihydro­anthracen-9-ol
title_full 9-[3-(Dimethyl­amino)­prop­yl]-10,10-dimethyl-9,10-dihydro­anthracen-9-ol
title_fullStr 9-[3-(Dimethyl­amino)­prop­yl]-10,10-dimethyl-9,10-dihydro­anthracen-9-ol
title_full_unstemmed 9-[3-(Dimethyl­amino)­prop­yl]-10,10-dimethyl-9,10-dihydro­anthracen-9-ol
title_short 9-[3-(Dimethyl­amino)­prop­yl]-10,10-dimethyl-9,10-dihydro­anthracen-9-ol
title_sort 9-[3-(dimethyl­amino)­prop­yl]-10,10-dimethyl-9,10-dihydro­anthracen-9-ol
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3569237/
https://www.ncbi.nlm.nih.gov/pubmed/23424460
http://dx.doi.org/10.1107/S1600536812050088
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