3,3′,5,5′-Tetra-tert-butyl-2′-hy­droxy-[1,1′-biphen­yl]-2-yl 4-methyl­benzene­sulfonate

In the title mol­ecule, C(37)H(48)O(4)S, the benzene rings in the biphenyl fragment are inclined to each other at 61.1 (1)°. The hy­droxy group is involved in a weak intra­molecular O—H⋯O(sulfonate) hydrogen bond. One tert-butyl group is disodered over two orientations in a 0.682 (17):0.318 (17) rat...

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Detalles Bibliográficos
Autores principales: Jian, Chunli, Zhang, Jinjin, Wang, Lei, Tang, Ning, Wu, Jincai
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3569248/
https://www.ncbi.nlm.nih.gov/pubmed/23424471
http://dx.doi.org/10.1107/S1600536812051938
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author Jian, Chunli
Zhang, Jinjin
Wang, Lei
Tang, Ning
Wu, Jincai
author_facet Jian, Chunli
Zhang, Jinjin
Wang, Lei
Tang, Ning
Wu, Jincai
author_sort Jian, Chunli
collection PubMed
description In the title mol­ecule, C(37)H(48)O(4)S, the benzene rings in the biphenyl fragment are inclined to each other at 61.1 (1)°. The hy­droxy group is involved in a weak intra­molecular O—H⋯O(sulfonate) hydrogen bond. One tert-butyl group is disodered over two orientations in a 0.682 (17):0.318 (17) ratio. In the crystal, weak C—H⋯O hydrogen bonds link the mol­ecules into columns in direction [100].
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spelling pubmed-35692482013-02-19 3,3′,5,5′-Tetra-tert-butyl-2′-hy­droxy-[1,1′-biphen­yl]-2-yl 4-methyl­benzene­sulfonate Jian, Chunli Zhang, Jinjin Wang, Lei Tang, Ning Wu, Jincai Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title mol­ecule, C(37)H(48)O(4)S, the benzene rings in the biphenyl fragment are inclined to each other at 61.1 (1)°. The hy­droxy group is involved in a weak intra­molecular O—H⋯O(sulfonate) hydrogen bond. One tert-butyl group is disodered over two orientations in a 0.682 (17):0.318 (17) ratio. In the crystal, weak C—H⋯O hydrogen bonds link the mol­ecules into columns in direction [100]. International Union of Crystallography 2013-01-04 /pmc/articles/PMC3569248/ /pubmed/23424471 http://dx.doi.org/10.1107/S1600536812051938 Text en © Jian et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Jian, Chunli
Zhang, Jinjin
Wang, Lei
Tang, Ning
Wu, Jincai
3,3′,5,5′-Tetra-tert-butyl-2′-hy­droxy-[1,1′-biphen­yl]-2-yl 4-methyl­benzene­sulfonate
title 3,3′,5,5′-Tetra-tert-butyl-2′-hy­droxy-[1,1′-biphen­yl]-2-yl 4-methyl­benzene­sulfonate
title_full 3,3′,5,5′-Tetra-tert-butyl-2′-hy­droxy-[1,1′-biphen­yl]-2-yl 4-methyl­benzene­sulfonate
title_fullStr 3,3′,5,5′-Tetra-tert-butyl-2′-hy­droxy-[1,1′-biphen­yl]-2-yl 4-methyl­benzene­sulfonate
title_full_unstemmed 3,3′,5,5′-Tetra-tert-butyl-2′-hy­droxy-[1,1′-biphen­yl]-2-yl 4-methyl­benzene­sulfonate
title_short 3,3′,5,5′-Tetra-tert-butyl-2′-hy­droxy-[1,1′-biphen­yl]-2-yl 4-methyl­benzene­sulfonate
title_sort 3,3′,5,5′-tetra-tert-butyl-2′-hy­droxy-[1,1′-biphen­yl]-2-yl 4-methyl­benzene­sulfonate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3569248/
https://www.ncbi.nlm.nih.gov/pubmed/23424471
http://dx.doi.org/10.1107/S1600536812051938
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