2-(Naphthalene-2-sulfonamido)-3-phenyl­propanoic acid

In the title compound, C(19)H(17)NO(4)S, the phenyl ring and the naphthalene ring system are oriented at a dihedral angle of 4.12 (2)° and the mol­ecule adopts a U-shaped conformation. The C(c)—C—N—S (c = carb­oxy) torsion angle is 90.98 (15)°. In the crystal, mol­ecules are linked by O—H⋯O and N—H⋯...

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Autores principales: Mubashar-ur-Rehman, Hafiz, Arshad, Muhammad Nadeem, Asiri, Abdullah M., Khan, Islam Ullah, Bilal, Muhammad
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3569255/
https://www.ncbi.nlm.nih.gov/pubmed/23424478
http://dx.doi.org/10.1107/S1600536813000081
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author Mubashar-ur-Rehman, Hafiz
Arshad, Muhammad Nadeem
Asiri, Abdullah M.
Khan, Islam Ullah
Bilal, Muhammad
author_facet Mubashar-ur-Rehman, Hafiz
Arshad, Muhammad Nadeem
Asiri, Abdullah M.
Khan, Islam Ullah
Bilal, Muhammad
author_sort Mubashar-ur-Rehman, Hafiz
collection PubMed
description In the title compound, C(19)H(17)NO(4)S, the phenyl ring and the naphthalene ring system are oriented at a dihedral angle of 4.12 (2)° and the mol­ecule adopts a U-shaped conformation. The C(c)—C—N—S (c = carb­oxy) torsion angle is 90.98 (15)°. In the crystal, mol­ecules are linked by O—H⋯O and N—H⋯O hydrogen bonds, resulting in (100) chains incorporating centrosymmetric R (2) (2)(14) and R (2) (2)(10) loops. Weak aromatic π–π stacking is also observed [centroid–centroid separations = 3.963 (2) and 3.932 (2) Å].
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spelling pubmed-35692552013-02-19 2-(Naphthalene-2-sulfonamido)-3-phenyl­propanoic acid Mubashar-ur-Rehman, Hafiz Arshad, Muhammad Nadeem Asiri, Abdullah M. Khan, Islam Ullah Bilal, Muhammad Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(19)H(17)NO(4)S, the phenyl ring and the naphthalene ring system are oriented at a dihedral angle of 4.12 (2)° and the mol­ecule adopts a U-shaped conformation. The C(c)—C—N—S (c = carb­oxy) torsion angle is 90.98 (15)°. In the crystal, mol­ecules are linked by O—H⋯O and N—H⋯O hydrogen bonds, resulting in (100) chains incorporating centrosymmetric R (2) (2)(14) and R (2) (2)(10) loops. Weak aromatic π–π stacking is also observed [centroid–centroid separations = 3.963 (2) and 3.932 (2) Å]. International Union of Crystallography 2013-01-09 /pmc/articles/PMC3569255/ /pubmed/23424478 http://dx.doi.org/10.1107/S1600536813000081 Text en © Mubashar-ur-Rehman et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Mubashar-ur-Rehman, Hafiz
Arshad, Muhammad Nadeem
Asiri, Abdullah M.
Khan, Islam Ullah
Bilal, Muhammad
2-(Naphthalene-2-sulfonamido)-3-phenyl­propanoic acid
title 2-(Naphthalene-2-sulfonamido)-3-phenyl­propanoic acid
title_full 2-(Naphthalene-2-sulfonamido)-3-phenyl­propanoic acid
title_fullStr 2-(Naphthalene-2-sulfonamido)-3-phenyl­propanoic acid
title_full_unstemmed 2-(Naphthalene-2-sulfonamido)-3-phenyl­propanoic acid
title_short 2-(Naphthalene-2-sulfonamido)-3-phenyl­propanoic acid
title_sort 2-(naphthalene-2-sulfonamido)-3-phenyl­propanoic acid
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3569255/
https://www.ncbi.nlm.nih.gov/pubmed/23424478
http://dx.doi.org/10.1107/S1600536813000081
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