N-(5-Amino-1H-1,2,4-triazol-3-yl)pyridine-2-carboxamide

The title compound, C(8)H(8)N(6)O, was obtained by the reaction of 3,5-diamino-1,2,4-triazole with ethyl 2-picolinate in a glass oven. The dihedral angles formed between the plane of the amide group and the pyridine and triazole rings are 11.8 (3) and 5.8 (3)°, respectively. In the crystal, an exten...

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Detalles Bibliográficos
Autores principales: Hernández-Gil, Javier, Ferrer, Sacramento, Ballesteros, Rafael, Castiñeiras, Alfonso
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3569762/
https://www.ncbi.nlm.nih.gov/pubmed/23424508
http://dx.doi.org/10.1107/S1600536813000123
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author Hernández-Gil, Javier
Ferrer, Sacramento
Ballesteros, Rafael
Castiñeiras, Alfonso
author_facet Hernández-Gil, Javier
Ferrer, Sacramento
Ballesteros, Rafael
Castiñeiras, Alfonso
author_sort Hernández-Gil, Javier
collection PubMed
description The title compound, C(8)H(8)N(6)O, was obtained by the reaction of 3,5-diamino-1,2,4-triazole with ethyl 2-picolinate in a glass oven. The dihedral angles formed between the plane of the amide group and the pyridine and triazole rings are 11.8 (3) and 5.8 (3)°, respectively. In the crystal, an extensive system of classical N—H⋯N and N—H⋯O hydrogen bonds generate an infinite three-dimensional network.
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spelling pubmed-35697622013-02-19 N-(5-Amino-1H-1,2,4-triazol-3-yl)pyridine-2-carboxamide Hernández-Gil, Javier Ferrer, Sacramento Ballesteros, Rafael Castiñeiras, Alfonso Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(8)H(8)N(6)O, was obtained by the reaction of 3,5-diamino-1,2,4-triazole with ethyl 2-picolinate in a glass oven. The dihedral angles formed between the plane of the amide group and the pyridine and triazole rings are 11.8 (3) and 5.8 (3)°, respectively. In the crystal, an extensive system of classical N—H⋯N and N—H⋯O hydrogen bonds generate an infinite three-dimensional network. International Union of Crystallography 2013-01-12 /pmc/articles/PMC3569762/ /pubmed/23424508 http://dx.doi.org/10.1107/S1600536813000123 Text en © Hernández-Gil et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Hernández-Gil, Javier
Ferrer, Sacramento
Ballesteros, Rafael
Castiñeiras, Alfonso
N-(5-Amino-1H-1,2,4-triazol-3-yl)pyridine-2-carboxamide
title N-(5-Amino-1H-1,2,4-triazol-3-yl)pyridine-2-carboxamide
title_full N-(5-Amino-1H-1,2,4-triazol-3-yl)pyridine-2-carboxamide
title_fullStr N-(5-Amino-1H-1,2,4-triazol-3-yl)pyridine-2-carboxamide
title_full_unstemmed N-(5-Amino-1H-1,2,4-triazol-3-yl)pyridine-2-carboxamide
title_short N-(5-Amino-1H-1,2,4-triazol-3-yl)pyridine-2-carboxamide
title_sort n-(5-amino-1h-1,2,4-triazol-3-yl)pyridine-2-carboxamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3569762/
https://www.ncbi.nlm.nih.gov/pubmed/23424508
http://dx.doi.org/10.1107/S1600536813000123
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AT castineirasalfonso n5amino1h124triazol3ylpyridine2carboxamide

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