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Sagittal focusing of synchrotron radiation X-rays using a winged crystal
A Si(111) winged crystal has been designed to minimize anticlastic bending and improve sagittal focusing efficiency. The crystal was thin with wide stiffening wings. The length-to-width ratio of the crystal was optimized by finite element analysis, and the optimal value was larger than the ‘golden v...
Autores principales: | , , , , , , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2013
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3573870/ https://www.ncbi.nlm.nih.gov/pubmed/23412477 http://dx.doi.org/10.1107/S0909049512049813 |
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author | Nisawa, A. Yoneda, Y. Ueno, G. Murakami, H. Okajima, Y. Yamamoto, K. Senba, Y. Uesugi, K. Tanaka, Y. Yamamoto, M. Goto, S. Ishikawa, T. |
author_facet | Nisawa, A. Yoneda, Y. Ueno, G. Murakami, H. Okajima, Y. Yamamoto, K. Senba, Y. Uesugi, K. Tanaka, Y. Yamamoto, M. Goto, S. Ishikawa, T. |
author_sort | Nisawa, A. |
collection | PubMed |
description | A Si(111) winged crystal has been designed to minimize anticlastic bending and improve sagittal focusing efficiency. The crystal was thin with wide stiffening wings. The length-to-width ratio of the crystal was optimized by finite element analysis, and the optimal value was larger than the ‘golden value’. The analysis showed that the slope error owing to anticlastic bending is less than the Darwin width. The X-rays were focused two-dimensionally using the crystal and a tangentially bent mirror. The observed profiles of the focal spot agreed well with the results of a ray-tracing calculation in the energy range from 8 to 17.5 keV. X-ray diffraction measurements with a high signal-to-noise ratio using this focusing system were demonstrated for a small protein crystal. |
format | Online Article Text |
id | pubmed-3573870 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2013 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-35738702013-03-06 Sagittal focusing of synchrotron radiation X-rays using a winged crystal Nisawa, A. Yoneda, Y. Ueno, G. Murakami, H. Okajima, Y. Yamamoto, K. Senba, Y. Uesugi, K. Tanaka, Y. Yamamoto, M. Goto, S. Ishikawa, T. J Synchrotron Radiat Research Papers A Si(111) winged crystal has been designed to minimize anticlastic bending and improve sagittal focusing efficiency. The crystal was thin with wide stiffening wings. The length-to-width ratio of the crystal was optimized by finite element analysis, and the optimal value was larger than the ‘golden value’. The analysis showed that the slope error owing to anticlastic bending is less than the Darwin width. The X-rays were focused two-dimensionally using the crystal and a tangentially bent mirror. The observed profiles of the focal spot agreed well with the results of a ray-tracing calculation in the energy range from 8 to 17.5 keV. X-ray diffraction measurements with a high signal-to-noise ratio using this focusing system were demonstrated for a small protein crystal. International Union of Crystallography 2013-03-01 2013-01-23 /pmc/articles/PMC3573870/ /pubmed/23412477 http://dx.doi.org/10.1107/S0909049512049813 Text en © A. Nisawa et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Research Papers Nisawa, A. Yoneda, Y. Ueno, G. Murakami, H. Okajima, Y. Yamamoto, K. Senba, Y. Uesugi, K. Tanaka, Y. Yamamoto, M. Goto, S. Ishikawa, T. Sagittal focusing of synchrotron radiation X-rays using a winged crystal |
title | Sagittal focusing of synchrotron radiation X-rays using a winged crystal |
title_full | Sagittal focusing of synchrotron radiation X-rays using a winged crystal |
title_fullStr | Sagittal focusing of synchrotron radiation X-rays using a winged crystal |
title_full_unstemmed | Sagittal focusing of synchrotron radiation X-rays using a winged crystal |
title_short | Sagittal focusing of synchrotron radiation X-rays using a winged crystal |
title_sort | sagittal focusing of synchrotron radiation x-rays using a winged crystal |
topic | Research Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3573870/ https://www.ncbi.nlm.nih.gov/pubmed/23412477 http://dx.doi.org/10.1107/S0909049512049813 |
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