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Sagittal focusing of synchrotron radiation X-rays using a winged crystal

A Si(111) winged crystal has been designed to minimize anticlastic bending and improve sagittal focusing efficiency. The crystal was thin with wide stiffening wings. The length-to-width ratio of the crystal was optimized by finite element analysis, and the optimal value was larger than the ‘golden v...

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Autores principales: Nisawa, A., Yoneda, Y., Ueno, G., Murakami, H., Okajima, Y., Yamamoto, K., Senba, Y., Uesugi, K., Tanaka, Y., Yamamoto, M., Goto, S., Ishikawa, T.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3573870/
https://www.ncbi.nlm.nih.gov/pubmed/23412477
http://dx.doi.org/10.1107/S0909049512049813
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author Nisawa, A.
Yoneda, Y.
Ueno, G.
Murakami, H.
Okajima, Y.
Yamamoto, K.
Senba, Y.
Uesugi, K.
Tanaka, Y.
Yamamoto, M.
Goto, S.
Ishikawa, T.
author_facet Nisawa, A.
Yoneda, Y.
Ueno, G.
Murakami, H.
Okajima, Y.
Yamamoto, K.
Senba, Y.
Uesugi, K.
Tanaka, Y.
Yamamoto, M.
Goto, S.
Ishikawa, T.
author_sort Nisawa, A.
collection PubMed
description A Si(111) winged crystal has been designed to minimize anticlastic bending and improve sagittal focusing efficiency. The crystal was thin with wide stiffening wings. The length-to-width ratio of the crystal was optimized by finite element analysis, and the optimal value was larger than the ‘golden value’. The analysis showed that the slope error owing to anticlastic bending is less than the Darwin width. The X-rays were focused two-dimensionally using the crystal and a tangentially bent mirror. The observed profiles of the focal spot agreed well with the results of a ray-tracing calculation in the energy range from 8 to 17.5 keV. X-ray diffraction measurements with a high signal-to-noise ratio using this focusing system were demonstrated for a small protein crystal.
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spelling pubmed-35738702013-03-06 Sagittal focusing of synchrotron radiation X-rays using a winged crystal Nisawa, A. Yoneda, Y. Ueno, G. Murakami, H. Okajima, Y. Yamamoto, K. Senba, Y. Uesugi, K. Tanaka, Y. Yamamoto, M. Goto, S. Ishikawa, T. J Synchrotron Radiat Research Papers A Si(111) winged crystal has been designed to minimize anticlastic bending and improve sagittal focusing efficiency. The crystal was thin with wide stiffening wings. The length-to-width ratio of the crystal was optimized by finite element analysis, and the optimal value was larger than the ‘golden value’. The analysis showed that the slope error owing to anticlastic bending is less than the Darwin width. The X-rays were focused two-dimensionally using the crystal and a tangentially bent mirror. The observed profiles of the focal spot agreed well with the results of a ray-tracing calculation in the energy range from 8 to 17.5 keV. X-ray diffraction measurements with a high signal-to-noise ratio using this focusing system were demonstrated for a small protein crystal. International Union of Crystallography 2013-03-01 2013-01-23 /pmc/articles/PMC3573870/ /pubmed/23412477 http://dx.doi.org/10.1107/S0909049512049813 Text en © A. Nisawa et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Papers
Nisawa, A.
Yoneda, Y.
Ueno, G.
Murakami, H.
Okajima, Y.
Yamamoto, K.
Senba, Y.
Uesugi, K.
Tanaka, Y.
Yamamoto, M.
Goto, S.
Ishikawa, T.
Sagittal focusing of synchrotron radiation X-rays using a winged crystal
title Sagittal focusing of synchrotron radiation X-rays using a winged crystal
title_full Sagittal focusing of synchrotron radiation X-rays using a winged crystal
title_fullStr Sagittal focusing of synchrotron radiation X-rays using a winged crystal
title_full_unstemmed Sagittal focusing of synchrotron radiation X-rays using a winged crystal
title_short Sagittal focusing of synchrotron radiation X-rays using a winged crystal
title_sort sagittal focusing of synchrotron radiation x-rays using a winged crystal
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3573870/
https://www.ncbi.nlm.nih.gov/pubmed/23412477
http://dx.doi.org/10.1107/S0909049512049813
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