(E)-2-Phenyl-N-tosyl­non-2-en-4-ynamide

The mol­ecule of the title compound, C(22)H(23)NO(3)S, adopts an E conformation about the C=C bond. The dihedral angle between the benzene rings is 23.79 (5)°. In the crystal, pairs of N—H⋯O hydrogen bonds link the mol­ecules, forming inversion dimers. The terminal butyl group is disordered over two...

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Detalles Bibliográficos
Autores principales: Meng, Xiang-Zhen, Wan, Xin-Jun
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588246/
https://www.ncbi.nlm.nih.gov/pubmed/23476459
http://dx.doi.org/10.1107/S1600536812048489
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author Meng, Xiang-Zhen
Wan, Xin-Jun
author_facet Meng, Xiang-Zhen
Wan, Xin-Jun
author_sort Meng, Xiang-Zhen
collection PubMed
description The mol­ecule of the title compound, C(22)H(23)NO(3)S, adopts an E conformation about the C=C bond. The dihedral angle between the benzene rings is 23.79 (5)°. In the crystal, pairs of N—H⋯O hydrogen bonds link the mol­ecules, forming inversion dimers. The terminal butyl group is disordered over two sets of sites in a 0.559 (6):0.441 (6) ratio.
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spelling pubmed-35882462013-03-08 (E)-2-Phenyl-N-tosyl­non-2-en-4-ynamide Meng, Xiang-Zhen Wan, Xin-Jun Acta Crystallogr Sect E Struct Rep Online Organic Papers The mol­ecule of the title compound, C(22)H(23)NO(3)S, adopts an E conformation about the C=C bond. The dihedral angle between the benzene rings is 23.79 (5)°. In the crystal, pairs of N—H⋯O hydrogen bonds link the mol­ecules, forming inversion dimers. The terminal butyl group is disordered over two sets of sites in a 0.559 (6):0.441 (6) ratio. International Union of Crystallography 2012-12-12 /pmc/articles/PMC3588246/ /pubmed/23476459 http://dx.doi.org/10.1107/S1600536812048489 Text en © Meng and Wan 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Meng, Xiang-Zhen
Wan, Xin-Jun
(E)-2-Phenyl-N-tosyl­non-2-en-4-ynamide
title (E)-2-Phenyl-N-tosyl­non-2-en-4-ynamide
title_full (E)-2-Phenyl-N-tosyl­non-2-en-4-ynamide
title_fullStr (E)-2-Phenyl-N-tosyl­non-2-en-4-ynamide
title_full_unstemmed (E)-2-Phenyl-N-tosyl­non-2-en-4-ynamide
title_short (E)-2-Phenyl-N-tosyl­non-2-en-4-ynamide
title_sort (e)-2-phenyl-n-tosyl­non-2-en-4-ynamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588246/
https://www.ncbi.nlm.nih.gov/pubmed/23476459
http://dx.doi.org/10.1107/S1600536812048489
work_keys_str_mv AT mengxiangzhen e2phenylntosylnon2en4ynamide
AT wanxinjun e2phenylntosylnon2en4ynamide

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