8-Hy­droxy-5,7-dimethyl­quinolin-1-ium hydrogen sulfate

The quinoline ring system of the title salt, C(11)H(12)NO(+)·HSO(4) (−), is essentially planar, with a maximum deviation of 0.054 (2) Å for all non H atoms. In the crystal, the cations and anions are linked via N—H⋯O, O—H⋯O and weak C—H⋯O hydrogen bonds, and are stacked respectively in columns along...

Descripción completa

Detalles Bibliográficos
Autores principales: Thanigaimani, Kaliyaperumal, Khalib, Nuridayanti Che, Arshad, Suhana, Razak, Ibrahim Abdul
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588270/
https://www.ncbi.nlm.nih.gov/pubmed/23476427
http://dx.doi.org/10.1107/S1600536812049483
_version_ 1782261527329374208
author Thanigaimani, Kaliyaperumal
Khalib, Nuridayanti Che
Arshad, Suhana
Razak, Ibrahim Abdul
author_facet Thanigaimani, Kaliyaperumal
Khalib, Nuridayanti Che
Arshad, Suhana
Razak, Ibrahim Abdul
author_sort Thanigaimani, Kaliyaperumal
collection PubMed
description The quinoline ring system of the title salt, C(11)H(12)NO(+)·HSO(4) (−), is essentially planar, with a maximum deviation of 0.054 (2) Å for all non H atoms. In the crystal, the cations and anions are linked via N—H⋯O, O—H⋯O and weak C—H⋯O hydrogen bonds, and are stacked respectively in columns along the a axis. π–π stacking inter­actions, with centroid–centroid distances of 3.5473 (12) and 3.6926 (12) Å, are also observed. The crystal studied was an inversion twin with refined components of 0.43 (7):0.57 (7).
format Online
Article
Text
id pubmed-3588270
institution National Center for Biotechnology Information
language English
publishDate 2012
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-35882702013-03-08 8-Hy­droxy-5,7-dimethyl­quinolin-1-ium hydrogen sulfate Thanigaimani, Kaliyaperumal Khalib, Nuridayanti Che Arshad, Suhana Razak, Ibrahim Abdul Acta Crystallogr Sect E Struct Rep Online Organic Papers The quinoline ring system of the title salt, C(11)H(12)NO(+)·HSO(4) (−), is essentially planar, with a maximum deviation of 0.054 (2) Å for all non H atoms. In the crystal, the cations and anions are linked via N—H⋯O, O—H⋯O and weak C—H⋯O hydrogen bonds, and are stacked respectively in columns along the a axis. π–π stacking inter­actions, with centroid–centroid distances of 3.5473 (12) and 3.6926 (12) Å, are also observed. The crystal studied was an inversion twin with refined components of 0.43 (7):0.57 (7). International Union of Crystallography 2012-12-08 /pmc/articles/PMC3588270/ /pubmed/23476427 http://dx.doi.org/10.1107/S1600536812049483 Text en © Thanigaimani et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Thanigaimani, Kaliyaperumal
Khalib, Nuridayanti Che
Arshad, Suhana
Razak, Ibrahim Abdul
8-Hy­droxy-5,7-dimethyl­quinolin-1-ium hydrogen sulfate
title 8-Hy­droxy-5,7-dimethyl­quinolin-1-ium hydrogen sulfate
title_full 8-Hy­droxy-5,7-dimethyl­quinolin-1-ium hydrogen sulfate
title_fullStr 8-Hy­droxy-5,7-dimethyl­quinolin-1-ium hydrogen sulfate
title_full_unstemmed 8-Hy­droxy-5,7-dimethyl­quinolin-1-ium hydrogen sulfate
title_short 8-Hy­droxy-5,7-dimethyl­quinolin-1-ium hydrogen sulfate
title_sort 8-hy­droxy-5,7-dimethyl­quinolin-1-ium hydrogen sulfate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588270/
https://www.ncbi.nlm.nih.gov/pubmed/23476427
http://dx.doi.org/10.1107/S1600536812049483
work_keys_str_mv AT thanigaimanikaliyaperumal 8hydroxy57dimethylquinolin1iumhydrogensulfate
AT khalibnuridayantiche 8hydroxy57dimethylquinolin1iumhydrogensulfate
AT arshadsuhana 8hydroxy57dimethylquinolin1iumhydrogensulfate
AT razakibrahimabdul 8hydroxy57dimethylquinolin1iumhydrogensulfate

Ejemplares similares