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2-[1-(2-Hydroxy-6-methoxyphenyl)ethylidene]-N-methylhydrazinecarbothioamide acetonitrile monosolvate
In the title compound, C(11)H(15)N(3)O(2)S·C(2)H(3)N, the dihedral angle between the benzene ring and the mean plane of the hydrazinecarbothioamide group is 75.1 (2)°. In the crystal, the main molecule is linked to the solvent molecule by a weak N—H⋯N hydrogen bond while O—H⋯S hydrogen bonds link...
| Autores principales: | , , , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2012
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588304/ https://www.ncbi.nlm.nih.gov/pubmed/23476372 http://dx.doi.org/10.1107/S1600536812048799 |
| _version_ | 1782261535075205120 |
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| author | Anderson, Brian J. Keeler, Alexander M. O’Rourke, Kelly A. Krauss, Shannon T. Jasinski, Jerry P. |
| author_facet | Anderson, Brian J. Keeler, Alexander M. O’Rourke, Kelly A. Krauss, Shannon T. Jasinski, Jerry P. |
| author_sort | Anderson, Brian J. |
| collection | PubMed |
| description | In the title compound, C(11)H(15)N(3)O(2)S·C(2)H(3)N, the dihedral angle between the benzene ring and the mean plane of the hydrazinecarbothioamide group is 75.1 (2)°. In the crystal, the main molecule is linked to the solvent molecule by a weak N—H⋯N hydrogen bond while O—H⋯S hydrogen bonds link the molecules into columns along [100]. |
| format | Online Article Text |
| id | pubmed-3588304 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2012 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-35883042013-03-08 2-[1-(2-Hydroxy-6-methoxyphenyl)ethylidene]-N-methylhydrazinecarbothioamide acetonitrile monosolvate Anderson, Brian J. Keeler, Alexander M. O’Rourke, Kelly A. Krauss, Shannon T. Jasinski, Jerry P. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(11)H(15)N(3)O(2)S·C(2)H(3)N, the dihedral angle between the benzene ring and the mean plane of the hydrazinecarbothioamide group is 75.1 (2)°. In the crystal, the main molecule is linked to the solvent molecule by a weak N—H⋯N hydrogen bond while O—H⋯S hydrogen bonds link the molecules into columns along [100]. International Union of Crystallography 2012-12-05 /pmc/articles/PMC3588304/ /pubmed/23476372 http://dx.doi.org/10.1107/S1600536812048799 Text en © Anderson et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Organic Papers Anderson, Brian J. Keeler, Alexander M. O’Rourke, Kelly A. Krauss, Shannon T. Jasinski, Jerry P. 2-[1-(2-Hydroxy-6-methoxyphenyl)ethylidene]-N-methylhydrazinecarbothioamide acetonitrile monosolvate |
| title | 2-[1-(2-Hydroxy-6-methoxyphenyl)ethylidene]-N-methylhydrazinecarbothioamide acetonitrile monosolvate |
| title_full | 2-[1-(2-Hydroxy-6-methoxyphenyl)ethylidene]-N-methylhydrazinecarbothioamide acetonitrile monosolvate |
| title_fullStr | 2-[1-(2-Hydroxy-6-methoxyphenyl)ethylidene]-N-methylhydrazinecarbothioamide acetonitrile monosolvate |
| title_full_unstemmed | 2-[1-(2-Hydroxy-6-methoxyphenyl)ethylidene]-N-methylhydrazinecarbothioamide acetonitrile monosolvate |
| title_short | 2-[1-(2-Hydroxy-6-methoxyphenyl)ethylidene]-N-methylhydrazinecarbothioamide acetonitrile monosolvate |
| title_sort | 2-[1-(2-hydroxy-6-methoxyphenyl)ethylidene]-n-methylhydrazinecarbothioamide acetonitrile monosolvate |
| topic | Organic Papers |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588304/ https://www.ncbi.nlm.nih.gov/pubmed/23476372 http://dx.doi.org/10.1107/S1600536812048799 |
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