(9H-Fluoren-9-yl)(phen­yl)phosphinic acid

The crystal structure of the title compound, C(19)H(15)O(2)P, features pairs of mol­ecules joined by O—H⋯O hydrogen bonds across crystallographic inversion centers. In addition, π–π inter­actions, with a centroid–centroid distance of 3.6273 (9) Å between the fluorene ring systems, connect the dimers...

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Detalles Bibliográficos
Autores principales: Burrow, Robert A., Siqueira da Silva, Rubia M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588309/
https://www.ncbi.nlm.nih.gov/pubmed/23476362
http://dx.doi.org/10.1107/S160053681204891X
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author Burrow, Robert A.
Siqueira da Silva, Rubia M.
author_facet Burrow, Robert A.
Siqueira da Silva, Rubia M.
author_sort Burrow, Robert A.
collection PubMed
description The crystal structure of the title compound, C(19)H(15)O(2)P, features pairs of mol­ecules joined by O—H⋯O hydrogen bonds across crystallographic inversion centers. In addition, π–π inter­actions, with a centroid–centroid distance of 3.6273 (9) Å between the fluorene ring systems, connect the dimers into chains along [01-1]. The three rings make dihedral angles of 1.34 (9), 1.52 (10) and 1.51 (7)° with each other.
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spelling pubmed-35883092013-03-08 (9H-Fluoren-9-yl)(phen­yl)phosphinic acid Burrow, Robert A. Siqueira da Silva, Rubia M. Acta Crystallogr Sect E Struct Rep Online Organic Papers The crystal structure of the title compound, C(19)H(15)O(2)P, features pairs of mol­ecules joined by O—H⋯O hydrogen bonds across crystallographic inversion centers. In addition, π–π inter­actions, with a centroid–centroid distance of 3.6273 (9) Å between the fluorene ring systems, connect the dimers into chains along [01-1]. The three rings make dihedral angles of 1.34 (9), 1.52 (10) and 1.51 (7)° with each other. International Union of Crystallography 2012-12-05 /pmc/articles/PMC3588309/ /pubmed/23476362 http://dx.doi.org/10.1107/S160053681204891X Text en © Burrow and Siqueira da Silva 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Burrow, Robert A.
Siqueira da Silva, Rubia M.
(9H-Fluoren-9-yl)(phen­yl)phosphinic acid
title (9H-Fluoren-9-yl)(phen­yl)phosphinic acid
title_full (9H-Fluoren-9-yl)(phen­yl)phosphinic acid
title_fullStr (9H-Fluoren-9-yl)(phen­yl)phosphinic acid
title_full_unstemmed (9H-Fluoren-9-yl)(phen­yl)phosphinic acid
title_short (9H-Fluoren-9-yl)(phen­yl)phosphinic acid
title_sort (9h-fluoren-9-yl)(phen­yl)phosphinic acid
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588309/
https://www.ncbi.nlm.nih.gov/pubmed/23476362
http://dx.doi.org/10.1107/S160053681204891X
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