2,2-Dimethyl-5-(2-nitro­benzyl­idene)-1,3-dioxane-4,6-dione

The asymmetric unit of the title compound, C(13)H(11)NO(6), contains two mol­ecules in both of which the six-membered 1,3-dioxane-4,6-dione ring shows a screw-boat conformation. The dihedral angles between the best planes through the six-membered rings are 47.8 (2) and 49.8 (2)°. In the crystal, C—H...

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Autores principales: García-Álvarez, Fernando, Romero, Nancy, Lobato-García, Carlos E., Terán, Joel L., Mendoza, Angel
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588381/
https://www.ncbi.nlm.nih.gov/pubmed/23476434
http://dx.doi.org/10.1107/S1600536812049677
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author García-Álvarez, Fernando
Romero, Nancy
Lobato-García, Carlos E.
Terán, Joel L.
Mendoza, Angel
author_facet García-Álvarez, Fernando
Romero, Nancy
Lobato-García, Carlos E.
Terán, Joel L.
Mendoza, Angel
author_sort García-Álvarez, Fernando
collection PubMed
description The asymmetric unit of the title compound, C(13)H(11)NO(6), contains two mol­ecules in both of which the six-membered 1,3-dioxane-4,6-dione ring shows a screw-boat conformation. The dihedral angles between the best planes through the six-membered rings are 47.8 (2) and 49.8 (2)°. In the crystal, C—H⋯O inter­actions link the mol­ecules, building a supramolecular sheet parallel to the c axis.
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spelling pubmed-35883812013-03-08 2,2-Dimethyl-5-(2-nitro­benzyl­idene)-1,3-dioxane-4,6-dione García-Álvarez, Fernando Romero, Nancy Lobato-García, Carlos E. Terán, Joel L. Mendoza, Angel Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(13)H(11)NO(6), contains two mol­ecules in both of which the six-membered 1,3-dioxane-4,6-dione ring shows a screw-boat conformation. The dihedral angles between the best planes through the six-membered rings are 47.8 (2) and 49.8 (2)°. In the crystal, C—H⋯O inter­actions link the mol­ecules, building a supramolecular sheet parallel to the c axis. International Union of Crystallography 2012-12-08 /pmc/articles/PMC3588381/ /pubmed/23476434 http://dx.doi.org/10.1107/S1600536812049677 Text en © García-Álvarez et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
García-Álvarez, Fernando
Romero, Nancy
Lobato-García, Carlos E.
Terán, Joel L.
Mendoza, Angel
2,2-Dimethyl-5-(2-nitro­benzyl­idene)-1,3-dioxane-4,6-dione
title 2,2-Dimethyl-5-(2-nitro­benzyl­idene)-1,3-dioxane-4,6-dione
title_full 2,2-Dimethyl-5-(2-nitro­benzyl­idene)-1,3-dioxane-4,6-dione
title_fullStr 2,2-Dimethyl-5-(2-nitro­benzyl­idene)-1,3-dioxane-4,6-dione
title_full_unstemmed 2,2-Dimethyl-5-(2-nitro­benzyl­idene)-1,3-dioxane-4,6-dione
title_short 2,2-Dimethyl-5-(2-nitro­benzyl­idene)-1,3-dioxane-4,6-dione
title_sort 2,2-dimethyl-5-(2-nitro­benzyl­idene)-1,3-dioxane-4,6-dione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588381/
https://www.ncbi.nlm.nih.gov/pubmed/23476434
http://dx.doi.org/10.1107/S1600536812049677
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