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N′-[(E)-2,3-Dihydroxybenzylidene]-2-methoxybenzohydrazide
The title compound, C(15)H(14)N(2)O(4) adopts an E conformation about the azomethine double bond. Intramolecular N—H⋯O and O—H⋯N hydrogen bonds generate S(6) rings and help to establish the molecular conformation. The dihedral angle between the benzene rings is 17.84 (10)°. In the crystal, molecul...
Autores principales: | , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2012
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588810/ https://www.ncbi.nlm.nih.gov/pubmed/23468775 http://dx.doi.org/10.1107/S1600536812042390 |
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author | Taha, Muhammad Baharudin, M. Syukri. Ismail, Nor Hadiani Shah, Syed Adnan Ali Yousuf, Sammer |
author_facet | Taha, Muhammad Baharudin, M. Syukri. Ismail, Nor Hadiani Shah, Syed Adnan Ali Yousuf, Sammer |
author_sort | Taha, Muhammad |
collection | PubMed |
description | The title compound, C(15)H(14)N(2)O(4) adopts an E conformation about the azomethine double bond. Intramolecular N—H⋯O and O—H⋯N hydrogen bonds generate S(6) rings and help to establish the molecular conformation. The dihedral angle between the benzene rings is 17.84 (10)°. In the crystal, molecules are linked by O—H⋯O and C—H⋯O hydrogen bonds into a two-dimensional network with a herring-bone pattern arranged parallel to the bc plane. |
format | Online Article Text |
id | pubmed-3588810 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2012 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-35888102013-03-06 N′-[(E)-2,3-Dihydroxybenzylidene]-2-methoxybenzohydrazide Taha, Muhammad Baharudin, M. Syukri. Ismail, Nor Hadiani Shah, Syed Adnan Ali Yousuf, Sammer Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(15)H(14)N(2)O(4) adopts an E conformation about the azomethine double bond. Intramolecular N—H⋯O and O—H⋯N hydrogen bonds generate S(6) rings and help to establish the molecular conformation. The dihedral angle between the benzene rings is 17.84 (10)°. In the crystal, molecules are linked by O—H⋯O and C—H⋯O hydrogen bonds into a two-dimensional network with a herring-bone pattern arranged parallel to the bc plane. International Union of Crystallography 2012-11-03 /pmc/articles/PMC3588810/ /pubmed/23468775 http://dx.doi.org/10.1107/S1600536812042390 Text en © Taha et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Taha, Muhammad Baharudin, M. Syukri. Ismail, Nor Hadiani Shah, Syed Adnan Ali Yousuf, Sammer N′-[(E)-2,3-Dihydroxybenzylidene]-2-methoxybenzohydrazide |
title |
N′-[(E)-2,3-Dihydroxybenzylidene]-2-methoxybenzohydrazide |
title_full |
N′-[(E)-2,3-Dihydroxybenzylidene]-2-methoxybenzohydrazide |
title_fullStr |
N′-[(E)-2,3-Dihydroxybenzylidene]-2-methoxybenzohydrazide |
title_full_unstemmed |
N′-[(E)-2,3-Dihydroxybenzylidene]-2-methoxybenzohydrazide |
title_short |
N′-[(E)-2,3-Dihydroxybenzylidene]-2-methoxybenzohydrazide |
title_sort | n′-[(e)-2,3-dihydroxybenzylidene]-2-methoxybenzohydrazide |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588810/ https://www.ncbi.nlm.nih.gov/pubmed/23468775 http://dx.doi.org/10.1107/S1600536812042390 |
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