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17-Hy­droxy-1,8-dimethyl-17-aza­penta­cyclo­[6.6.5.0(2,7).0(9,14).0(15,19)]nona­deca-2,4,6,9(14),10,12-hexa­ene-16,18-dione

In the title compound, C(20)H(17)NO(3) (alternative name: N-hy­droxy-9,10-dimethyl-9,10-ethano­anthracene-11,12-dicarboximide), the rigid ethano­anthracene-dicarboximide moiety has a roof-shaped geometry, the inter­planar angle between the two terminal phenyl rings being 124.9 (6)°. In the crystal,...

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Autores principales: Miroslaw, Barbara, Koziol, Anna E., Pakosinska-Parys, Magdalena, Struga, Marta
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588838/
https://www.ncbi.nlm.nih.gov/pubmed/23468803
http://dx.doi.org/10.1107/S1600536812045151
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author Miroslaw, Barbara
Koziol, Anna E.
Pakosinska-Parys, Magdalena
Struga, Marta
author_facet Miroslaw, Barbara
Koziol, Anna E.
Pakosinska-Parys, Magdalena
Struga, Marta
author_sort Miroslaw, Barbara
collection PubMed
description In the title compound, C(20)H(17)NO(3) (alternative name: N-hy­droxy-9,10-dimethyl-9,10-ethano­anthracene-11,12-dicarboximide), the rigid ethano­anthracene-dicarboximide moiety has a roof-shaped geometry, the inter­planar angle between the two terminal phenyl rings being 124.9 (6)°. In the crystal, mol­ecules are linked via O—H⋯O hydrogen bonds, forming chains along [010]. C—H⋯O and C—H⋯π inter­actions link adjacent chains, leading to the formation of a three-dimensional structure.
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spelling pubmed-35888382013-03-06 17-Hy­droxy-1,8-dimethyl-17-aza­penta­cyclo­[6.6.5.0(2,7).0(9,14).0(15,19)]nona­deca-2,4,6,9(14),10,12-hexa­ene-16,18-dione Miroslaw, Barbara Koziol, Anna E. Pakosinska-Parys, Magdalena Struga, Marta Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(20)H(17)NO(3) (alternative name: N-hy­droxy-9,10-dimethyl-9,10-ethano­anthracene-11,12-dicarboximide), the rigid ethano­anthracene-dicarboximide moiety has a roof-shaped geometry, the inter­planar angle between the two terminal phenyl rings being 124.9 (6)°. In the crystal, mol­ecules are linked via O—H⋯O hydrogen bonds, forming chains along [010]. C—H⋯O and C—H⋯π inter­actions link adjacent chains, leading to the formation of a three-dimensional structure. International Union of Crystallography 2012-11-07 /pmc/articles/PMC3588838/ /pubmed/23468803 http://dx.doi.org/10.1107/S1600536812045151 Text en © Miroslaw et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Miroslaw, Barbara
Koziol, Anna E.
Pakosinska-Parys, Magdalena
Struga, Marta
17-Hy­droxy-1,8-dimethyl-17-aza­penta­cyclo­[6.6.5.0(2,7).0(9,14).0(15,19)]nona­deca-2,4,6,9(14),10,12-hexa­ene-16,18-dione
title 17-Hy­droxy-1,8-dimethyl-17-aza­penta­cyclo­[6.6.5.0(2,7).0(9,14).0(15,19)]nona­deca-2,4,6,9(14),10,12-hexa­ene-16,18-dione
title_full 17-Hy­droxy-1,8-dimethyl-17-aza­penta­cyclo­[6.6.5.0(2,7).0(9,14).0(15,19)]nona­deca-2,4,6,9(14),10,12-hexa­ene-16,18-dione
title_fullStr 17-Hy­droxy-1,8-dimethyl-17-aza­penta­cyclo­[6.6.5.0(2,7).0(9,14).0(15,19)]nona­deca-2,4,6,9(14),10,12-hexa­ene-16,18-dione
title_full_unstemmed 17-Hy­droxy-1,8-dimethyl-17-aza­penta­cyclo­[6.6.5.0(2,7).0(9,14).0(15,19)]nona­deca-2,4,6,9(14),10,12-hexa­ene-16,18-dione
title_short 17-Hy­droxy-1,8-dimethyl-17-aza­penta­cyclo­[6.6.5.0(2,7).0(9,14).0(15,19)]nona­deca-2,4,6,9(14),10,12-hexa­ene-16,18-dione
title_sort 17-hy­droxy-1,8-dimethyl-17-aza­penta­cyclo­[6.6.5.0(2,7).0(9,14).0(15,19)]nona­deca-2,4,6,9(14),10,12-hexa­ene-16,18-dione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588838/
https://www.ncbi.nlm.nih.gov/pubmed/23468803
http://dx.doi.org/10.1107/S1600536812045151
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