4-Chloro-6-meth­oxy­pyrimidin-2-amine–succinic acid (2/1)

The asymmetric unit of the title compound, 2C(5)H(6)ClN(3)O·C(4)H(6)O(4), consists of one 4-chloro-6-meth­oxy­pyrimidin-2-amine mol­ecule and one half-mol­ecule of succinic acid which lies about an inversion centre. In the crystal, the acid and base mol­ecules are linked through N—H⋯O and O—H⋯N hydr...

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Autores principales: Thanigaimani, Kaliyaperumal, Khalib, Nuridayanti Che, Arshad, Suhana, Razak, Ibrahim Abdul
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588944/
https://www.ncbi.nlm.nih.gov/pubmed/23476180
http://dx.doi.org/10.1107/S1600536812046156
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author Thanigaimani, Kaliyaperumal
Khalib, Nuridayanti Che
Arshad, Suhana
Razak, Ibrahim Abdul
author_facet Thanigaimani, Kaliyaperumal
Khalib, Nuridayanti Che
Arshad, Suhana
Razak, Ibrahim Abdul
author_sort Thanigaimani, Kaliyaperumal
collection PubMed
description The asymmetric unit of the title compound, 2C(5)H(6)ClN(3)O·C(4)H(6)O(4), consists of one 4-chloro-6-meth­oxy­pyrimidin-2-amine mol­ecule and one half-mol­ecule of succinic acid which lies about an inversion centre. In the crystal, the acid and base mol­ecules are linked through N—H⋯O and O—H⋯N hydrogen bonds, forming a tape along [1-10] in which R (2) (2)(8) and R (4) (2)(8) hydrogen-bond motifs are observed. The tapes are further inter­linked through a pair of C—H⋯O hydrogen bonds into a sheet parallel to (11-2).
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spelling pubmed-35889442013-03-08 4-Chloro-6-meth­oxy­pyrimidin-2-amine–succinic acid (2/1) Thanigaimani, Kaliyaperumal Khalib, Nuridayanti Che Arshad, Suhana Razak, Ibrahim Abdul Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, 2C(5)H(6)ClN(3)O·C(4)H(6)O(4), consists of one 4-chloro-6-meth­oxy­pyrimidin-2-amine mol­ecule and one half-mol­ecule of succinic acid which lies about an inversion centre. In the crystal, the acid and base mol­ecules are linked through N—H⋯O and O—H⋯N hydrogen bonds, forming a tape along [1-10] in which R (2) (2)(8) and R (4) (2)(8) hydrogen-bond motifs are observed. The tapes are further inter­linked through a pair of C—H⋯O hydrogen bonds into a sheet parallel to (11-2). International Union of Crystallography 2012-11-14 /pmc/articles/PMC3588944/ /pubmed/23476180 http://dx.doi.org/10.1107/S1600536812046156 Text en © Thanigaimani et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Thanigaimani, Kaliyaperumal
Khalib, Nuridayanti Che
Arshad, Suhana
Razak, Ibrahim Abdul
4-Chloro-6-meth­oxy­pyrimidin-2-amine–succinic acid (2/1)
title 4-Chloro-6-meth­oxy­pyrimidin-2-amine–succinic acid (2/1)
title_full 4-Chloro-6-meth­oxy­pyrimidin-2-amine–succinic acid (2/1)
title_fullStr 4-Chloro-6-meth­oxy­pyrimidin-2-amine–succinic acid (2/1)
title_full_unstemmed 4-Chloro-6-meth­oxy­pyrimidin-2-amine–succinic acid (2/1)
title_short 4-Chloro-6-meth­oxy­pyrimidin-2-amine–succinic acid (2/1)
title_sort 4-chloro-6-meth­oxy­pyrimidin-2-amine–succinic acid (2/1)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588944/
https://www.ncbi.nlm.nih.gov/pubmed/23476180
http://dx.doi.org/10.1107/S1600536812046156
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AT arshadsuhana 4chloro6methoxypyrimidin2aminesuccinicacid21
AT razakibrahimabdul 4chloro6methoxypyrimidin2aminesuccinicacid21

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