4-Phenyl-1H-1,5-benzodiazepin-2(3H)-one

In the title compound, C(15)H(12)N(2)O, the phenyl ring makes a dihedral angle of 32.45 (9)° with the benzene ring of the 1,5-benzodiazepin-2-one unit. The seven-membered ring adopts a boat conformation with the methyl­ene group as the prow and the fused benzene-ring C atoms as the stern. In the cry...

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Detalles Bibliográficos
Autores principales: Akkurt, Mehmet, Kennedy, Alan R., Younes, Sabry H. H., Mohamed, Shaaban K., Abdelhamid, Antar A.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588955/
https://www.ncbi.nlm.nih.gov/pubmed/23476191
http://dx.doi.org/10.1107/S160053681204651X
Descripción
Sumario:In the title compound, C(15)H(12)N(2)O, the phenyl ring makes a dihedral angle of 32.45 (9)° with the benzene ring of the 1,5-benzodiazepin-2-one unit. The seven-membered ring adopts a boat conformation with the methyl­ene group as the prow and the fused benzene-ring C atoms as the stern. In the crystal, inversion dimers linked by pairs of N—H⋯O hydrogen bonds generate R (2) (2)(8) loops. The dimers are further linked by C—H⋯O hydrogen bonds, so forming a column along the a-axis direction.

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