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Morpholine–4-nitro­phenol (1/2)

In the title adduct, 2C(6)H(5)NO(3)·C(4)H(9)NO, the morpholine ring adopts a chair conformation. The dihedral angle between the two nitro­phenol rings is 69.47 (9)°. The nitro groups attached to the benzene rings make dihedral angles of 3.37 (16) and 3.14 (13)° in the two mol­ecules of nitro­phenol....

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Detalles Bibliográficos
Autores principales: Muralidharan, Srinivasan, Vidyalakshmi, Yechuri, Srinivasan, Thothadri, Gopalakrishnan, Rengasamy, Velmurugan, Devadasan
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588998/
https://www.ncbi.nlm.nih.gov/pubmed/23476234
http://dx.doi.org/10.1107/S1600536812047174
Descripción
Sumario:In the title adduct, 2C(6)H(5)NO(3)·C(4)H(9)NO, the morpholine ring adopts a chair conformation. The dihedral angle between the two nitro­phenol rings is 69.47 (9)°. The nitro groups attached to the benzene rings make dihedral angles of 3.37 (16) and 3.14 (13)° in the two mol­ecules of nitro­phenol. The crystal structure is stabilized by N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds and further consolidated by C—H⋯O inter­actions, resulting in a three-dimensional network.