Cargando…
Morpholine–4-nitrophenol (1/2)
In the title adduct, 2C(6)H(5)NO(3)·C(4)H(9)NO, the morpholine ring adopts a chair conformation. The dihedral angle between the two nitrophenol rings is 69.47 (9)°. The nitro groups attached to the benzene rings make dihedral angles of 3.37 (16) and 3.14 (13)° in the two molecules of nitrophenol....
| Autores principales: | , , , , |
|---|---|
| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2012
|
| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588998/ https://www.ncbi.nlm.nih.gov/pubmed/23476234 http://dx.doi.org/10.1107/S1600536812047174 |
| _version_ | 1782261674295689216 |
|---|---|
| author | Muralidharan, Srinivasan Vidyalakshmi, Yechuri Srinivasan, Thothadri Gopalakrishnan, Rengasamy Velmurugan, Devadasan |
| author_facet | Muralidharan, Srinivasan Vidyalakshmi, Yechuri Srinivasan, Thothadri Gopalakrishnan, Rengasamy Velmurugan, Devadasan |
| author_sort | Muralidharan, Srinivasan |
| collection | PubMed |
| description | In the title adduct, 2C(6)H(5)NO(3)·C(4)H(9)NO, the morpholine ring adopts a chair conformation. The dihedral angle between the two nitrophenol rings is 69.47 (9)°. The nitro groups attached to the benzene rings make dihedral angles of 3.37 (16) and 3.14 (13)° in the two molecules of nitrophenol. The crystal structure is stabilized by N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds and further consolidated by C—H⋯O interactions, resulting in a three-dimensional network. |
| format | Online Article Text |
| id | pubmed-3588998 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2012 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-35889982013-03-08 Morpholine–4-nitrophenol (1/2) Muralidharan, Srinivasan Vidyalakshmi, Yechuri Srinivasan, Thothadri Gopalakrishnan, Rengasamy Velmurugan, Devadasan Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title adduct, 2C(6)H(5)NO(3)·C(4)H(9)NO, the morpholine ring adopts a chair conformation. The dihedral angle between the two nitrophenol rings is 69.47 (9)°. The nitro groups attached to the benzene rings make dihedral angles of 3.37 (16) and 3.14 (13)° in the two molecules of nitrophenol. The crystal structure is stabilized by N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds and further consolidated by C—H⋯O interactions, resulting in a three-dimensional network. International Union of Crystallography 2012-11-24 /pmc/articles/PMC3588998/ /pubmed/23476234 http://dx.doi.org/10.1107/S1600536812047174 Text en © Muralidharan et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Organic Papers Muralidharan, Srinivasan Vidyalakshmi, Yechuri Srinivasan, Thothadri Gopalakrishnan, Rengasamy Velmurugan, Devadasan Morpholine–4-nitrophenol (1/2) |
| title | Morpholine–4-nitrophenol (1/2) |
| title_full | Morpholine–4-nitrophenol (1/2) |
| title_fullStr | Morpholine–4-nitrophenol (1/2) |
| title_full_unstemmed | Morpholine–4-nitrophenol (1/2) |
| title_short | Morpholine–4-nitrophenol (1/2) |
| title_sort | morpholine–4-nitrophenol (1/2) |
| topic | Organic Papers |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3588998/ https://www.ncbi.nlm.nih.gov/pubmed/23476234 http://dx.doi.org/10.1107/S1600536812047174 |
| work_keys_str_mv | AT muralidharansrinivasan morpholine4nitrophenol12 AT vidyalakshmiyechuri morpholine4nitrophenol12 AT srinivasanthothadri morpholine4nitrophenol12 AT gopalakrishnanrengasamy morpholine4nitrophenol12 AT velmurugandevadasan morpholine4nitrophenol12 |