Bis(4-sulfamoylanilinium) sulfate

In the title salt, 2C(6)H(9)N(2)O(2)S(+)·SO(4) (2−), the sulfate S atom is situated on a crystallographic twofold axis (the symmetry of the anion is 2). The anion exerts intense libration, which is manifested by shortening of the observed sulfate S—O bonds, as well as by features in the electron-den...

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Detalles Bibliográficos
Autores principales: Ravikumar, B., Pandiarajan, S., Athimoolam, S.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3629637/
https://www.ncbi.nlm.nih.gov/pubmed/23634124
http://dx.doi.org/10.1107/S1600536813007216
Descripción
Sumario:In the title salt, 2C(6)H(9)N(2)O(2)S(+)·SO(4) (2−), the sulfate S atom is situated on a crystallographic twofold axis (the symmetry of the anion is 2). The anion exerts intense libration, which is manifested by shortening of the observed sulfate S—O bonds, as well as by features in the electron-density map. The crystal structure is stabilized through a three-dimensional hydrogen-bonding network formed by strong N—H⋯O hydrogen bonds.

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