Bis(4-sulfamoylanilinium) sulfate

In the title salt, 2C(6)H(9)N(2)O(2)S(+)·SO(4) (2−), the sulfate S atom is situated on a crystallographic twofold axis (the symmetry of the anion is 2). The anion exerts intense libration, which is manifested by shortening of the observed sulfate S—O bonds, as well as by features in the electron-den...

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Detalles Bibliográficos
Autores principales: Ravikumar, B., Pandiarajan, S., Athimoolam, S.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3629637/
https://www.ncbi.nlm.nih.gov/pubmed/23634124
http://dx.doi.org/10.1107/S1600536813007216
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author Ravikumar, B.
Pandiarajan, S.
Athimoolam, S.
author_facet Ravikumar, B.
Pandiarajan, S.
Athimoolam, S.
author_sort Ravikumar, B.
collection PubMed
description In the title salt, 2C(6)H(9)N(2)O(2)S(+)·SO(4) (2−), the sulfate S atom is situated on a crystallographic twofold axis (the symmetry of the anion is 2). The anion exerts intense libration, which is manifested by shortening of the observed sulfate S—O bonds, as well as by features in the electron-density map. The crystal structure is stabilized through a three-dimensional hydrogen-bonding network formed by strong N—H⋯O hydrogen bonds.
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spelling pubmed-36296372013-04-30 Bis(4-sulfamoylanilinium) sulfate Ravikumar, B. Pandiarajan, S. Athimoolam, S. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title salt, 2C(6)H(9)N(2)O(2)S(+)·SO(4) (2−), the sulfate S atom is situated on a crystallographic twofold axis (the symmetry of the anion is 2). The anion exerts intense libration, which is manifested by shortening of the observed sulfate S—O bonds, as well as by features in the electron-density map. The crystal structure is stabilized through a three-dimensional hydrogen-bonding network formed by strong N—H⋯O hydrogen bonds. International Union of Crystallography 2013-03-28 /pmc/articles/PMC3629637/ /pubmed/23634124 http://dx.doi.org/10.1107/S1600536813007216 Text en © Ravikumar et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Ravikumar, B.
Pandiarajan, S.
Athimoolam, S.
Bis(4-sulfamoylanilinium) sulfate
title Bis(4-sulfamoylanilinium) sulfate
title_full Bis(4-sulfamoylanilinium) sulfate
title_fullStr Bis(4-sulfamoylanilinium) sulfate
title_full_unstemmed Bis(4-sulfamoylanilinium) sulfate
title_short Bis(4-sulfamoylanilinium) sulfate
title_sort bis(4-sulfamoylanilinium) sulfate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3629637/
https://www.ncbi.nlm.nih.gov/pubmed/23634124
http://dx.doi.org/10.1107/S1600536813007216
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AT pandiarajans bis4sulfamoylaniliniumsulfate
AT athimoolams bis4sulfamoylaniliniumsulfate

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