Ethyl 2-oxo-3-(3-phthalimidoprop­yl)-2,3-dihydro-1H-1,3-benzimidazole-1-carboxyl­ate

In the title compound, C(21)H(19)N(3)O(5), the phthalimide and benzamidazole ring systems are linked by a propyl chain. The benzamidazole unit also carries an eth­oxy­carbonyl substit­uent. The phthalimido and benzimidazole ring systems are essentially planar, the maximum deviations from their mean...

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Autores principales: Belaziz, Dounia, Kandri Rodi, Youssef, Kandri Rodi, Adiba, Essassi, El Mokhtar, Saadi, Mohamed, El Ammari, Lahcen
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3647841/
https://www.ncbi.nlm.nih.gov/pubmed/23723807
http://dx.doi.org/10.1107/S1600536813008325
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author Belaziz, Dounia
Kandri Rodi, Youssef
Kandri Rodi, Adiba
Essassi, El Mokhtar
Saadi, Mohamed
El Ammari, Lahcen
author_facet Belaziz, Dounia
Kandri Rodi, Youssef
Kandri Rodi, Adiba
Essassi, El Mokhtar
Saadi, Mohamed
El Ammari, Lahcen
author_sort Belaziz, Dounia
collection PubMed
description In the title compound, C(21)H(19)N(3)O(5), the phthalimide and benzamidazole ring systems are linked by a propyl chain. The benzamidazole unit also carries an eth­oxy­carbonyl substit­uent. The phthalimido and benzimidazole ring systems are essentially planar, the maximum deviations from their mean planes being 0.008 (2) and 0.020 (2) Å, respectively. The two ring systems are almost orthogonal to one another, making a dihedral angle of 82.37 (8)°. In the crystal, C—H⋯O hydrogen bonds and C—H⋯π contacts stack the mol­ecules along the b axis.
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spelling pubmed-36478412013-05-30 Ethyl 2-oxo-3-(3-phthalimidoprop­yl)-2,3-dihydro-1H-1,3-benzimidazole-1-carboxyl­ate Belaziz, Dounia Kandri Rodi, Youssef Kandri Rodi, Adiba Essassi, El Mokhtar Saadi, Mohamed El Ammari, Lahcen Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(21)H(19)N(3)O(5), the phthalimide and benzamidazole ring systems are linked by a propyl chain. The benzamidazole unit also carries an eth­oxy­carbonyl substit­uent. The phthalimido and benzimidazole ring systems are essentially planar, the maximum deviations from their mean planes being 0.008 (2) and 0.020 (2) Å, respectively. The two ring systems are almost orthogonal to one another, making a dihedral angle of 82.37 (8)°. In the crystal, C—H⋯O hydrogen bonds and C—H⋯π contacts stack the mol­ecules along the b axis. International Union of Crystallography 2013-04-05 /pmc/articles/PMC3647841/ /pubmed/23723807 http://dx.doi.org/10.1107/S1600536813008325 Text en © Belaziz et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Belaziz, Dounia
Kandri Rodi, Youssef
Kandri Rodi, Adiba
Essassi, El Mokhtar
Saadi, Mohamed
El Ammari, Lahcen
Ethyl 2-oxo-3-(3-phthalimidoprop­yl)-2,3-dihydro-1H-1,3-benzimidazole-1-carboxyl­ate
title Ethyl 2-oxo-3-(3-phthalimidoprop­yl)-2,3-dihydro-1H-1,3-benzimidazole-1-carboxyl­ate
title_full Ethyl 2-oxo-3-(3-phthalimidoprop­yl)-2,3-dihydro-1H-1,3-benzimidazole-1-carboxyl­ate
title_fullStr Ethyl 2-oxo-3-(3-phthalimidoprop­yl)-2,3-dihydro-1H-1,3-benzimidazole-1-carboxyl­ate
title_full_unstemmed Ethyl 2-oxo-3-(3-phthalimidoprop­yl)-2,3-dihydro-1H-1,3-benzimidazole-1-carboxyl­ate
title_short Ethyl 2-oxo-3-(3-phthalimidoprop­yl)-2,3-dihydro-1H-1,3-benzimidazole-1-carboxyl­ate
title_sort ethyl 2-oxo-3-(3-phthalimidoprop­yl)-2,3-dihydro-1h-1,3-benzimidazole-1-carboxyl­ate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3647841/
https://www.ncbi.nlm.nih.gov/pubmed/23723807
http://dx.doi.org/10.1107/S1600536813008325
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