Cargando…
3-(4-Methoxyphenyl)-1,3-selenazolo[2,3-b][1,3]benzothiazol-4-ium hydrogen sulfate
The title compound, C(16)H(12)NOSSe(+)·HSO(4) (−), was obtained from a mixture of 3-(4-methoxyphenyl)[1,3]selenazolo[2,3-b][1,3]benzothiazol-4-ium chloride and potassium hydrogen sulfate. In the cation, the benzene ring is twisted by 71.62 (7)° from the tricycle mean plane. In the crystal, O—H⋯...
| Autores principales: | , , , , |
|---|---|
| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2013
|
| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3648238/ https://www.ncbi.nlm.nih.gov/pubmed/23723858 http://dx.doi.org/10.1107/S1600536813009288 |
| _version_ | 1782268799736610816 |
|---|---|
| author | Mammadova, Gunay Z. Matsulevich, Zhanna V. Borisova, Galina N. Borisov, Alexander V. Khrustalev, Victor N. |
| author_facet | Mammadova, Gunay Z. Matsulevich, Zhanna V. Borisova, Galina N. Borisov, Alexander V. Khrustalev, Victor N. |
| author_sort | Mammadova, Gunay Z. |
| collection | PubMed |
| description | The title compound, C(16)H(12)NOSSe(+)·HSO(4) (−), was obtained from a mixture of 3-(4-methoxyphenyl)[1,3]selenazolo[2,3-b][1,3]benzothiazol-4-ium chloride and potassium hydrogen sulfate. In the cation, the benzene ring is twisted by 71.62 (7)° from the tricycle mean plane. In the crystal, O—H⋯O hydrogen bonds link the anions into chains along [100]. The anions in adjacent chains are linked via weak C—H⋯O hydrogen bonds. The crystal packing exhibits short intermolecular contacts between the chalcogen unit and the O atoms: Se⋯O(anion) 2.713 (3), Se⋯O(cation) 2.987 (3) and S⋯O(anion) 2.958 (3) Å. |
| format | Online Article Text |
| id | pubmed-3648238 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2013 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-36482382013-05-30 3-(4-Methoxyphenyl)-1,3-selenazolo[2,3-b][1,3]benzothiazol-4-ium hydrogen sulfate Mammadova, Gunay Z. Matsulevich, Zhanna V. Borisova, Galina N. Borisov, Alexander V. Khrustalev, Victor N. Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(16)H(12)NOSSe(+)·HSO(4) (−), was obtained from a mixture of 3-(4-methoxyphenyl)[1,3]selenazolo[2,3-b][1,3]benzothiazol-4-ium chloride and potassium hydrogen sulfate. In the cation, the benzene ring is twisted by 71.62 (7)° from the tricycle mean plane. In the crystal, O—H⋯O hydrogen bonds link the anions into chains along [100]. The anions in adjacent chains are linked via weak C—H⋯O hydrogen bonds. The crystal packing exhibits short intermolecular contacts between the chalcogen unit and the O atoms: Se⋯O(anion) 2.713 (3), Se⋯O(cation) 2.987 (3) and S⋯O(anion) 2.958 (3) Å. International Union of Crystallography 2013-04-13 /pmc/articles/PMC3648238/ /pubmed/23723858 http://dx.doi.org/10.1107/S1600536813009288 Text en © Mammadova et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Organic Papers Mammadova, Gunay Z. Matsulevich, Zhanna V. Borisova, Galina N. Borisov, Alexander V. Khrustalev, Victor N. 3-(4-Methoxyphenyl)-1,3-selenazolo[2,3-b][1,3]benzothiazol-4-ium hydrogen sulfate |
| title | 3-(4-Methoxyphenyl)-1,3-selenazolo[2,3-b][1,3]benzothiazol-4-ium hydrogen sulfate |
| title_full | 3-(4-Methoxyphenyl)-1,3-selenazolo[2,3-b][1,3]benzothiazol-4-ium hydrogen sulfate |
| title_fullStr | 3-(4-Methoxyphenyl)-1,3-selenazolo[2,3-b][1,3]benzothiazol-4-ium hydrogen sulfate |
| title_full_unstemmed | 3-(4-Methoxyphenyl)-1,3-selenazolo[2,3-b][1,3]benzothiazol-4-ium hydrogen sulfate |
| title_short | 3-(4-Methoxyphenyl)-1,3-selenazolo[2,3-b][1,3]benzothiazol-4-ium hydrogen sulfate |
| title_sort | 3-(4-methoxyphenyl)-1,3-selenazolo[2,3-b][1,3]benzothiazol-4-ium hydrogen sulfate |
| topic | Organic Papers |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3648238/ https://www.ncbi.nlm.nih.gov/pubmed/23723858 http://dx.doi.org/10.1107/S1600536813009288 |
| work_keys_str_mv | AT mammadovagunayz 34methoxyphenyl13selenazolo23b13benzothiazol4iumhydrogensulfate AT matsulevichzhannav 34methoxyphenyl13selenazolo23b13benzothiazol4iumhydrogensulfate AT borisovagalinan 34methoxyphenyl13selenazolo23b13benzothiazol4iumhydrogensulfate AT borisovalexanderv 34methoxyphenyl13selenazolo23b13benzothiazol4iumhydrogensulfate AT khrustalevvictorn 34methoxyphenyl13selenazolo23b13benzothiazol4iumhydrogensulfate |