8,15-Dioxa-10,13-di­aza­tetra­cyclo­[14.4.0.0(2,7).0(9,14)]icosa-1(16),2,4,6,9(14),10,12,17,19-nona­ene

The asymmetric unit of the title compound, C(16)H(10)N(2)O(2), contains one half-mol­ecule, the complete mol­ecule being generated by twofold rotation symmetry. The plane of the pyrazine ring forms a dihedral angle of 64.87 (6)° with that of the benzene ring, and the planes of the two benzene rings...

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Autores principales: Srinivasan, Thothadri, Kalpana, Venkatesan, Rajakumar, Perumal, Velmurugan, Devadasan
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3648330/
https://www.ncbi.nlm.nih.gov/pubmed/23723950
http://dx.doi.org/10.1107/S1600536813011318
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author Srinivasan, Thothadri
Kalpana, Venkatesan
Rajakumar, Perumal
Velmurugan, Devadasan
author_facet Srinivasan, Thothadri
Kalpana, Venkatesan
Rajakumar, Perumal
Velmurugan, Devadasan
author_sort Srinivasan, Thothadri
collection PubMed
description The asymmetric unit of the title compound, C(16)H(10)N(2)O(2), contains one half-mol­ecule, the complete mol­ecule being generated by twofold rotation symmetry. The plane of the pyrazine ring forms a dihedral angle of 64.87 (6)° with that of the benzene ring, and the planes of the two benzene rings are inclined to one another by 54.20 (6)°. The O atom deviates from the plane of the benzene ring by 0.1549 (8) Å. There are no significant inter­molecular inter­actions in the crystal.
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spelling pubmed-36483302013-05-30 8,15-Dioxa-10,13-di­aza­tetra­cyclo­[14.4.0.0(2,7).0(9,14)]icosa-1(16),2,4,6,9(14),10,12,17,19-nona­ene Srinivasan, Thothadri Kalpana, Venkatesan Rajakumar, Perumal Velmurugan, Devadasan Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(16)H(10)N(2)O(2), contains one half-mol­ecule, the complete mol­ecule being generated by twofold rotation symmetry. The plane of the pyrazine ring forms a dihedral angle of 64.87 (6)° with that of the benzene ring, and the planes of the two benzene rings are inclined to one another by 54.20 (6)°. The O atom deviates from the plane of the benzene ring by 0.1549 (8) Å. There are no significant inter­molecular inter­actions in the crystal. International Union of Crystallography 2013-04-30 /pmc/articles/PMC3648330/ /pubmed/23723950 http://dx.doi.org/10.1107/S1600536813011318 Text en © Srinivasan et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Srinivasan, Thothadri
Kalpana, Venkatesan
Rajakumar, Perumal
Velmurugan, Devadasan
8,15-Dioxa-10,13-di­aza­tetra­cyclo­[14.4.0.0(2,7).0(9,14)]icosa-1(16),2,4,6,9(14),10,12,17,19-nona­ene
title 8,15-Dioxa-10,13-di­aza­tetra­cyclo­[14.4.0.0(2,7).0(9,14)]icosa-1(16),2,4,6,9(14),10,12,17,19-nona­ene
title_full 8,15-Dioxa-10,13-di­aza­tetra­cyclo­[14.4.0.0(2,7).0(9,14)]icosa-1(16),2,4,6,9(14),10,12,17,19-nona­ene
title_fullStr 8,15-Dioxa-10,13-di­aza­tetra­cyclo­[14.4.0.0(2,7).0(9,14)]icosa-1(16),2,4,6,9(14),10,12,17,19-nona­ene
title_full_unstemmed 8,15-Dioxa-10,13-di­aza­tetra­cyclo­[14.4.0.0(2,7).0(9,14)]icosa-1(16),2,4,6,9(14),10,12,17,19-nona­ene
title_short 8,15-Dioxa-10,13-di­aza­tetra­cyclo­[14.4.0.0(2,7).0(9,14)]icosa-1(16),2,4,6,9(14),10,12,17,19-nona­ene
title_sort 8,15-dioxa-10,13-di­aza­tetra­cyclo­[14.4.0.0(2,7).0(9,14)]icosa-1(16),2,4,6,9(14),10,12,17,19-nona­ene
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3648330/
https://www.ncbi.nlm.nih.gov/pubmed/23723950
http://dx.doi.org/10.1107/S1600536813011318
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