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3-(Ammoniomethyl)pyridinium bis(perchlorate)
In the title molecular salt, C(6)H(10)N(2) (2+)·2ClO(4) (−), the Cl—O bond lengths [anion 1: 1.369 (3)–1.415 (3); anion 2: 1.420 (2)–1.441 (2) Å] and the O—Cl—O angles [anion 1: 105.4 (2)–111.8 (4); anion 2: 107.8 (1)–110.3 (1)°] indicate a slight distortion of the perchlorate anions from regular te...
| Autores principales: | , , , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2013
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3684928/ https://www.ncbi.nlm.nih.gov/pubmed/23795030 http://dx.doi.org/10.1107/S1600536813012038 |
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| author | Bayar, Imen Kefi, Riadh Sidonio Pereira da Silva, Pedro Ramos Silva, Manuela Ben Nasr, Cherif |
| author_facet | Bayar, Imen Kefi, Riadh Sidonio Pereira da Silva, Pedro Ramos Silva, Manuela Ben Nasr, Cherif |
| author_sort | Bayar, Imen |
| collection | PubMed |
| description | In the title molecular salt, C(6)H(10)N(2) (2+)·2ClO(4) (−), the Cl—O bond lengths [anion 1: 1.369 (3)–1.415 (3); anion 2: 1.420 (2)–1.441 (2) Å] and the O—Cl—O angles [anion 1: 105.4 (2)–111.8 (4); anion 2: 107.8 (1)–110.3 (1)°] indicate a slight distortion of the perchlorate anions from regular tetrahedral symmetry. In the crystal, the components are linked into columns along the a-axis direction via N—H⋯O and C—H⋯O hydrogen bonds, with stacks of the organic molecules being surrounded by stacks of perchlorate anions. |
| format | Online Article Text |
| id | pubmed-3684928 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2013 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-36849282013-06-21 3-(Ammoniomethyl)pyridinium bis(perchlorate) Bayar, Imen Kefi, Riadh Sidonio Pereira da Silva, Pedro Ramos Silva, Manuela Ben Nasr, Cherif Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title molecular salt, C(6)H(10)N(2) (2+)·2ClO(4) (−), the Cl—O bond lengths [anion 1: 1.369 (3)–1.415 (3); anion 2: 1.420 (2)–1.441 (2) Å] and the O—Cl—O angles [anion 1: 105.4 (2)–111.8 (4); anion 2: 107.8 (1)–110.3 (1)°] indicate a slight distortion of the perchlorate anions from regular tetrahedral symmetry. In the crystal, the components are linked into columns along the a-axis direction via N—H⋯O and C—H⋯O hydrogen bonds, with stacks of the organic molecules being surrounded by stacks of perchlorate anions. International Union of Crystallography 2013-05-11 /pmc/articles/PMC3684928/ /pubmed/23795030 http://dx.doi.org/10.1107/S1600536813012038 Text en © Bayar et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Organic Papers Bayar, Imen Kefi, Riadh Sidonio Pereira da Silva, Pedro Ramos Silva, Manuela Ben Nasr, Cherif 3-(Ammoniomethyl)pyridinium bis(perchlorate) |
| title | 3-(Ammoniomethyl)pyridinium bis(perchlorate) |
| title_full | 3-(Ammoniomethyl)pyridinium bis(perchlorate) |
| title_fullStr | 3-(Ammoniomethyl)pyridinium bis(perchlorate) |
| title_full_unstemmed | 3-(Ammoniomethyl)pyridinium bis(perchlorate) |
| title_short | 3-(Ammoniomethyl)pyridinium bis(perchlorate) |
| title_sort | 3-(ammoniomethyl)pyridinium bis(perchlorate) |
| topic | Organic Papers |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3684928/ https://www.ncbi.nlm.nih.gov/pubmed/23795030 http://dx.doi.org/10.1107/S1600536813012038 |
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