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N′-[(E)-2-Hy­droxy-5-meth­oxy­benzyl­idene]pyridine-4-carbohydrazide monohydrate

The title compound, C(14)H(13)N(3)O(3)·H(2)O, adopts an E conformation with respect to the azomethine bond and crystallizes in the amide form. An intra­molecular O—H⋯N hydrogen bond occurs. In the crystal, the lattice water molecule plays a major role in the supramolecular architecture by interconne...

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Autores principales: Prasanna, M. K., Sithambaresan, M., Pradeepkumar, K., Kurup, M. R. Prathapachandra
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3685038/
https://www.ncbi.nlm.nih.gov/pubmed/23795057
http://dx.doi.org/10.1107/S160053681301235X
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author Prasanna, M. K.
Sithambaresan, M.
Pradeepkumar, K.
Kurup, M. R. Prathapachandra
author_facet Prasanna, M. K.
Sithambaresan, M.
Pradeepkumar, K.
Kurup, M. R. Prathapachandra
author_sort Prasanna, M. K.
collection PubMed
description The title compound, C(14)H(13)N(3)O(3)·H(2)O, adopts an E conformation with respect to the azomethine bond and crystallizes in the amide form. An intra­molecular O—H⋯N hydrogen bond occurs. In the crystal, the lattice water molecule plays a major role in the supramolecular architecture by interconnecting adjacent molecules into a three-dimensional netwrok by means of O—H⋯O, O—H⋯N and N—H⋯O hydrogen-bonding inter­actions. The structure also features two non-classical C—H⋯O inter­actions.
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spelling pubmed-36850382013-06-21 N′-[(E)-2-Hy­droxy-5-meth­oxy­benzyl­idene]pyridine-4-carbohydrazide monohydrate Prasanna, M. K. Sithambaresan, M. Pradeepkumar, K. Kurup, M. R. Prathapachandra Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(13)N(3)O(3)·H(2)O, adopts an E conformation with respect to the azomethine bond and crystallizes in the amide form. An intra­molecular O—H⋯N hydrogen bond occurs. In the crystal, the lattice water molecule plays a major role in the supramolecular architecture by interconnecting adjacent molecules into a three-dimensional netwrok by means of O—H⋯O, O—H⋯N and N—H⋯O hydrogen-bonding inter­actions. The structure also features two non-classical C—H⋯O inter­actions. International Union of Crystallography 2013-05-15 /pmc/articles/PMC3685038/ /pubmed/23795057 http://dx.doi.org/10.1107/S160053681301235X Text en © Prasanna et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Prasanna, M. K.
Sithambaresan, M.
Pradeepkumar, K.
Kurup, M. R. Prathapachandra
N′-[(E)-2-Hy­droxy-5-meth­oxy­benzyl­idene]pyridine-4-carbohydrazide monohydrate
title N′-[(E)-2-Hy­droxy-5-meth­oxy­benzyl­idene]pyridine-4-carbohydrazide monohydrate
title_full N′-[(E)-2-Hy­droxy-5-meth­oxy­benzyl­idene]pyridine-4-carbohydrazide monohydrate
title_fullStr N′-[(E)-2-Hy­droxy-5-meth­oxy­benzyl­idene]pyridine-4-carbohydrazide monohydrate
title_full_unstemmed N′-[(E)-2-Hy­droxy-5-meth­oxy­benzyl­idene]pyridine-4-carbohydrazide monohydrate
title_short N′-[(E)-2-Hy­droxy-5-meth­oxy­benzyl­idene]pyridine-4-carbohydrazide monohydrate
title_sort n′-[(e)-2-hy­droxy-5-meth­oxy­benzyl­idene]pyridine-4-carbohydrazide monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3685038/
https://www.ncbi.nlm.nih.gov/pubmed/23795057
http://dx.doi.org/10.1107/S160053681301235X
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