3-{[5-(4-Chloro­phen­yl)-3-methyl-1H-pyrazol-1-yl]meth­yl}-4-m-tolyl-1H-1,2,4-triazole-5(4H)-thione

In the title compound, C(20)H(18)ClN(5)S, the toluene and triazole rings are oriented almost perpendicular to each other, making a dihedral angle of 89.97 (9)°, whereas the dihedral angle between cholorophenyl and pyrazole rings is 54.57 (11)°. In the crystal, pairs of N—H⋯N hydrogen bonds link the...

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Autores principales: Farrukh, Muhammad A., Ahmed, Maqsood, Mohamed, Shaaban K., Marzouk, Adel A., El-Moghazy, Samir M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2013
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3685083/
https://www.ncbi.nlm.nih.gov/pubmed/23795102
http://dx.doi.org/10.1107/S1600536813013494
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author Farrukh, Muhammad A.
Ahmed, Maqsood
Mohamed, Shaaban K.
Marzouk, Adel A.
El-Moghazy, Samir M.
author_facet Farrukh, Muhammad A.
Ahmed, Maqsood
Mohamed, Shaaban K.
Marzouk, Adel A.
El-Moghazy, Samir M.
author_sort Farrukh, Muhammad A.
collection PubMed
description In the title compound, C(20)H(18)ClN(5)S, the toluene and triazole rings are oriented almost perpendicular to each other, making a dihedral angle of 89.97 (9)°, whereas the dihedral angle between cholorophenyl and pyrazole rings is 54.57 (11)°. In the crystal, pairs of N—H⋯N hydrogen bonds link the mol­ecules into inversion dimers. Weaker C—H⋯S and C—H⋯Cl inter­actions are also present.
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spelling pubmed-36850832013-06-21 3-{[5-(4-Chloro­phen­yl)-3-methyl-1H-pyrazol-1-yl]meth­yl}-4-m-tolyl-1H-1,2,4-triazole-5(4H)-thione Farrukh, Muhammad A. Ahmed, Maqsood Mohamed, Shaaban K. Marzouk, Adel A. El-Moghazy, Samir M. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(20)H(18)ClN(5)S, the toluene and triazole rings are oriented almost perpendicular to each other, making a dihedral angle of 89.97 (9)°, whereas the dihedral angle between cholorophenyl and pyrazole rings is 54.57 (11)°. In the crystal, pairs of N—H⋯N hydrogen bonds link the mol­ecules into inversion dimers. Weaker C—H⋯S and C—H⋯Cl inter­actions are also present. International Union of Crystallography 2013-05-22 /pmc/articles/PMC3685083/ /pubmed/23795102 http://dx.doi.org/10.1107/S1600536813013494 Text en © Farrukh et al. 2013 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Farrukh, Muhammad A.
Ahmed, Maqsood
Mohamed, Shaaban K.
Marzouk, Adel A.
El-Moghazy, Samir M.
3-{[5-(4-Chloro­phen­yl)-3-methyl-1H-pyrazol-1-yl]meth­yl}-4-m-tolyl-1H-1,2,4-triazole-5(4H)-thione
title 3-{[5-(4-Chloro­phen­yl)-3-methyl-1H-pyrazol-1-yl]meth­yl}-4-m-tolyl-1H-1,2,4-triazole-5(4H)-thione
title_full 3-{[5-(4-Chloro­phen­yl)-3-methyl-1H-pyrazol-1-yl]meth­yl}-4-m-tolyl-1H-1,2,4-triazole-5(4H)-thione
title_fullStr 3-{[5-(4-Chloro­phen­yl)-3-methyl-1H-pyrazol-1-yl]meth­yl}-4-m-tolyl-1H-1,2,4-triazole-5(4H)-thione
title_full_unstemmed 3-{[5-(4-Chloro­phen­yl)-3-methyl-1H-pyrazol-1-yl]meth­yl}-4-m-tolyl-1H-1,2,4-triazole-5(4H)-thione
title_short 3-{[5-(4-Chloro­phen­yl)-3-methyl-1H-pyrazol-1-yl]meth­yl}-4-m-tolyl-1H-1,2,4-triazole-5(4H)-thione
title_sort 3-{[5-(4-chloro­phen­yl)-3-methyl-1h-pyrazol-1-yl]meth­yl}-4-m-tolyl-1h-1,2,4-triazole-5(4h)-thione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3685083/
https://www.ncbi.nlm.nih.gov/pubmed/23795102
http://dx.doi.org/10.1107/S1600536813013494
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